Emulsified nano-calcium carbonate as well as preparation method and application thereof
A nano-calcium carbonate and high-calcium technology, applied in the field of food additives, can solve the problems of affecting taste, gritty calcium, poor dispersibility, etc., and achieve the effects of simplifying the production process, reducing production costs, and good self-dispersion
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Embodiment 1
[0027] Embodiment 1, the preparation of emulsified nano calcium carbonate
[0028] Weigh 5.4g of nano-calcium carbonate (60-120nm in particle size) and add it into 20ml of pure water, and form a suspension by stirring.
[0029] Add 3g of gum arabic (molecular weight: 300,000 to 1,000,000 Daltons) into the above suspension, stir and disperse; stir and heat the above solution to 70°C, and continue stirring at this temperature for 30 minutes to obtain a dispersion.
[0030] The above dispersion is spray-dried (spray speed: 50m / s, temperature 190°C); that is, emulsified nano-calcium carbonate is obtained.
[0031] The electron micrograph of emulsified nano-calcium carbonate of the present invention is as figure 1 shown by figure 1 It can be seen that the diameter of the emulsified nano-calcium carbonate prepared in this embodiment is 20-80nm.
Embodiment 2
[0032] Embodiment 2, the preparation of emulsified nano calcium carbonate
[0033] The preparation steps are the same as in Example 1, except that the mass ratio of nano-calcium carbonate to gum arabic is 1.5:1, and the diameter of the prepared emulsified nano-calcium carbonate is 20-100 nm.
Embodiment 3
[0034] Embodiment 3, the dispersibility evaluation of emulsified nano calcium carbonate
[0035] The aqueous dispersion of the emulsified nano-calcium carbonate powder prepared by preparation examples 1 and 2 and P24 (the nano-active calcium carbonate (CCR-800CCR-805CCR-900) produced by Guangzhou Zhenwei Chemical Technology Co., Ltd.), such as figure 2 As shown in the left figure (where S 1 and S 2 Respectively represent the emulsified nano-calcium carbonate prepared by embodiment 1 and 2).
[0036] The dispersion after standing for 4 days is as follows: figure 2 shown in the figure on the right.
[0037] Depend on figure 2 It can be seen that the emulsified nano-calcium carbonate prepared by the present invention basically reaches the dispersion performance of P24.
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