Molybdenum alloy doped with aluminum oxide and preparation method thereof as well as molybdenum alloy wire
A molybdenum alloy and alumina technology, applied in the high temperature refractory field, can solve problems such as the limitation of raw material sources, and achieve the effects of good wear resistance and arc ablation resistance, high hardness and high wear resistance
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Embodiment 1
[0040] The molybdenum alloy doped with alumina in this example contains α-Al 2 o 3The mass percentage of nanoparticles is 0.10%, and the balance is Mo and unavoidable impurity elements.
[0041] The preparation method of the aluminum oxide-doped molybdenum alloy of the present embodiment is:
[0042] 1) Preparation of AlOOH nanoparticle suspension by hydrothermal method: In an autoclave with a capacity of 250mL, add 21.5g of aluminum nitrate and 5.5g of urea respectively, add 20mL of glycerol as template agent and dispersant, and then add distilled water 200mL, with a filling degree of 80%, heat the autoclave to 180°C, hold for 15 hours, after cooling, a suspension containing AlOOH nanoparticles with good dispersion is obtained, and set aside;
[0043] 2) Dissolve 5000g of ammonium tetramolybdate in distilled water, add ammonia water to adjust the pH value to 8~10, add enough distilled water to ensure that ammonium tetramolybdate is completely dissolved to form a solution, a...
Embodiment 2
[0049] The molybdenum alloy doped with alumina in this example contains α-Al 2 o 3 The mass percentage of nanoparticles is 0.20%, and the balance is Mo and unavoidable impurity elements.
[0050] The preparation method of the aluminum oxide-doped molybdenum alloy of the present embodiment is:
[0051] 1) Prepare AlOOH nanoparticles by hydrothermal method. In an autoclave with a capacity of 250mL, add 40.8g of aluminum nitrate and 10.0g of urea respectively, add 20mL of glycerol as template agent and dispersant, and then add 250mL of distilled water, The filling degree is 80%, the autoclave is heated to 180 ° C, and the holding time is 15 h. After cooling, a suspension containing AlOOH nanoparticles with good dispersion is obtained, and it is set aside;
[0052] 2) Dissolve 5000g of ammonium dimolybdate in distilled water, add ammonia water to adjust the pH value to 8~10, add enough distilled water to ensure that ammonium dimolybdate is completely dissolved to form a solution...
Embodiment 3
[0058] The molybdenum alloy doped with alumina in this example contains α-Al 2 o 3 The mass percentage of nanoparticles is 0.5%, and the balance is Mo and unavoidable impurity elements.
[0059] The preparation method of the aluminum oxide-doped molybdenum alloy of the present embodiment is:
[0060] 1) Prepare AlOOH nanoparticles by hydrothermal method. In an autoclave with a capacity of 500 mL, add 88.85 g of aluminum sulfate and 26.4 g of urea, add 40 mL of glycerol as a template agent and dispersant, and then add 500 mL of distilled water. The filling degree is 80%, the autoclave is heated to 180 ° C, the holding time is 15 h, and the AlOOH nanoparticle suspension is obtained after cooling, and it is set aside;
[0061] 2) Dissolve 5000g of ammonium heptamolybdate in distilled water, add ammonia water to adjust the pH value to 8~10, add enough distilled water to ensure that the ammonium heptamolybdate is completely dissolved to form a solution, and then add step 1) to th...
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