Protective film with heating-reducible adhesion and preparation method thereof
A protective film and adhesive technology, applied in the direction of adhesives, adhesive types, polyurea/polyurethane adhesives, etc., can solve the problems of low work efficiency, easy residues on the casing or screen, and manual tearing of protective films. , to achieve the effect of easy operation, simple preparation method and strong adhesion
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Embodiment 1
[0029] Components of the heating adhesive 2: 20% by weight of polyurethane resin, 10% by weight of MDI blocked isocyanate curing agent, 65% by weight of ketone organic solvent, and 5% by weight of Expandable microsphere foaming agent; wherein, the particle diameter of the self-expanding microsphere in the self-expanding microsphere foaming agent is 15 μm.
[0030] The preparation of heating viscosifying glue 2 comprises the following steps:
[0031] a) Add the ketone organic solvent and self-expanding microsphere foaming agent into the mixing tank for stirring, the stirring speed is 150r / min, and the stirring time is 30min.
[0032] b) adding polyurethane resin into the solution treated in step a), and stirring for 7 minutes.
[0033] c) Add an MDI blocked isocyanate curing agent into the mixing barrel in the solution treated in step b), and stir for 10 minutes, so as to prepare the heat-viscosity-reducing adhesive 2.
[0034] The preparation of the heat-reducing viscosity-r...
Embodiment 2
[0040] The components of the heating viscosifying adhesive 2: 55% by weight of polyester resin, 8% by weight of TDI blocked isocyanate curing agent, 30% by weight of benzene organic solvent, and 7% by weight of A self-expanding microsphere foaming agent; wherein, the particle diameter of the self-expanding microsphere in the self-expanding microsphere foaming agent is 20 μm.
[0041] The preparation of heating viscosifying glue 2 comprises the following steps:
[0042] a) Add benzene organic solvent and self-expanding microsphere foaming agent into the mixing tank for stirring, the stirring speed is 180r / min, and the stirring time is 25min.
[0043] b) adding polyester resin into the solution treated in step a), and stirring for 10 minutes.
[0044] c) Adding TDI blocked isocyanate curing agent into the solution treated in step b), and stirring for 8 minutes, so as to prepare heating viscosifying adhesive 2.
[0045] The preparation of the heat-reducing viscosity-reducing pr...
Embodiment 3
[0051] Components of the heating adhesive 2: 90% by weight of acrylic resin, 0.1% by weight of IPDI isocyanurate curing agent, 9% by weight of deionized water, and 0.9% by weight of A self-expanding microsphere foaming agent; wherein, the particle diameter of the self-expanding microsphere in the self-expanding microsphere foaming agent is 25 μm.
[0052] The preparation of heating viscosifying glue 2 comprises the following steps:
[0053] a) Add benzene organic solvent and self-expanding microsphere foaming agent into the mixing tank for stirring, the stirring speed is 200r / min, and the stirring time is 30min.
[0054] b) adding acrylic resin into the solution treated in step a), and stirring for 10 minutes.
[0055]c) Adding IPDI isocyanurate curing agent into the solution treated in step b), and stirring for 5 minutes, so as to prepare the heat-viscosity-reducing adhesive 2.
[0056] The preparation of the heat-reducing viscosity-reducing protective film comprises the fo...
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