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A kind of sodium pyroborate iron black crystalline glaze and preparation method thereof

A sodium pyroborate and crystalline glaze technology, applied in the field of ceramics, can solve the problems of single color, can not highlight the special artistic effect of ceramic color glaze artistic beauty, and achieve the effects of accurate process control, simple structure, and stable physical and chemical properties.

Active Publication Date: 2019-07-09
潮州市维欧陶瓷有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Ordinary ceramic colored glazes add metal colorants to the glass enamel to achieve color development during the firing process. Such glazes are often single in color and cannot highlight the artistic beauty of the ceramic colored glaze itself and the high-temperature firing process. Special artistic effects produced in

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A sodium pyroborate iron black crystalline glaze, the composition of raw materials includes: sodium pyroborate, potassium feldspar powder, silicon dioxide, lithium carbonate and ferric oxide; the mass percentage of each raw material component is: sodium pyroborate 35.5% , Potassium feldspar powder 21.5%, silicon dioxide 14.5%, lithium carbonate 6.6% and ferric oxide 21.9%.

[0028] A preparation method of sodium pyroborate iron black crystalline glaze, comprising the following steps:

[0029] (1) Carry out batching according to the raw material composition of sodium pyroborate iron black crystalline glaze, sodium pyroborate, potassium feldspar powder, silicon dioxide and lithium carbonate, add pure water, after mixing, join in the fast ball mill, the speed of the fast ball mill is 450rpm, ball milling time 3.5h, filter with a 400-mesh sieve to remove ungrinded impurities; wherein, by mass ratio, pure water: (sodium pyroborate+potassium feldspar powder+silica+lithium car...

Embodiment 2

[0032] A sodium pyroborate iron black crystalline glaze, the composition of its raw materials includes: sodium pyroborate, potassium feldspar powder, silicon dioxide, lithium carbonate, ferric oxide, manganese dioxide and cobalt oxide; the mass percentage of each raw material component It is: sodium pyroborate 35.5%, potassium feldspar powder 21.5%, silicon dioxide 14.5%, lithium carbonate 6.6%, ferric oxide 19%, manganese dioxide 1.9% and cobalt oxide 1%.

[0033] A preparation method of sodium pyroborate iron black crystalline glaze, comprising the following steps:

[0034] (1) According to the sodium pyroborate iron black crystalline glaze, add sodium pyroborate, potassium feldspar powder, silicon dioxide and lithium carbonate, pure water, after mixing, add to the fast ball mill, the speed of the fast ball mill is 450rpm, ball mill For 3.5 hours, filter with a 400-mesh sieve to remove ungrinded impurities; wherein, by mass ratio, pure water: (sodium pyroborate+potassium fel...

Embodiment 3

[0037] A sodium pyroborate iron black crystalline glaze, the composition of its raw materials includes: sodium pyroborate, potassium feldspar powder, silicon dioxide, lithium carbonate and ferric oxide; the mass percentage of each raw material component is: sodium pyroborate 38.5% , Potassium feldspar powder 25.5%, silicon dioxide 16.5%, lithium carbonate 7.6% and ferric oxide 11.9%.

[0038] A preparation method of sodium pyroborate iron black crystalline glaze, comprising the following steps:

[0039] (1) Carry out batching according to the raw material composition of sodium pyroborate iron black crystalline glaze, sodium pyroborate, potassium feldspar powder, silicon dioxide and lithium carbonate, add pure water, after mixing, join in the fast ball mill, the speed of the fast ball mill is 550rpm, ball milling time 3.5h, filter with a 400-mesh sieve to remove ungrinded impurities; wherein, by mass ratio, pure water: (sodium pyroborate+potassium feldspar powder+silica+lithium...

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PUM

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Abstract

The invention relates to a sodium pyroborate iron black crystalline glaze and a preparation method thereof, and belongs to the technical field of ceramics. The sodium pyroborate iron black crystalline glaze is prepared from the following raw material components in percentage by mass: 35.5 to 38.5 % of sodium pyroborate, 21.5 to 25.5% of potassium feldspar powder, 14.5 to 16.5% of silicon dioxide, 6.6 to 7.6% of lithium carbonate and 11.9 to 21.9% of ferric oxide; the sodium pyroborate iron black crystalline glaze can also be prepared from 1.9 to 2.5% of manganese dioxide and 1 to 1.5% of cobalt oxide. The sodium pyroborate iron black crystalline glaze has the advantages that the particular ceramic glaze art effect is realized, and the silver metal bright spot texture is formed on a black ceramic glaze surface; by adding the sodium pyroborate into the sodium pyroborate iron black crystalline glaze, the required amount of a melting agent is effectively reduced, and the amount of raw materials in the components is reduced; air bubbles on the glaze surface are also prevented by the sodium pyroborate; after long-time experiment at the temperature of minus 30 DEG C, the crack or falling of the glaze surface is avoided, and the corrosion by common acid and alkaline is resisted.

Description

technical field [0001] The invention relates to the technical field of ceramics, in particular to a sodium pyroborate iron black crystalline glaze and a preparation method thereof. Background technique [0002] Ceramic glaze is an important raw material that must be used in the production of ceramics. It has a strong protective effect on the ceramic body. At the same time, the physical properties of silicate make the glass enamel on the ceramic surface effectively resistant to acid and alkali corrosion. Very good antibacterial properties. Ordinary ceramic color glazes are achieved by adding metal colorants to the glass enamel to achieve color development during the firing process. Such glaze colors are often single in color and cannot highlight the artistic beauty of the ceramic color glaze itself and the high-temperature firing process. special artistic effects produced in Sodium pyroborate iron black crystalline glaze effectively overcomes the deficiencies of ceramic gla...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C03C8/14
CPCC03C8/14
Inventor 沈海泳王灿平
Owner 潮州市维欧陶瓷有限公司
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