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High-strength and high-toughness ceramic composite and preparation thereof

A technology for ceramic composite materials and raw materials, applied in the field of materials, can solve problems such as toughness to be improved, and achieve the effects of simple preparation method, high strength and toughness

Active Publication Date: 2017-02-15
江西新宏信陶瓷有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The toughness of existing ceramic composites needs to be improved

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Example 1: Preparation of ceramic composite materials

[0020] Weight ratio of raw materials: nano titanium carbide, 40 parts; nano titanium nitride, 35 parts; nano silicon carbide, 30 parts; calcite powder, 10 parts; modified nano illite, 10 parts; deionized water, 10 parts; minerals Oil, 8 parts; Silane coupling agent KH560, 4 parts; Fumaric acid, 3 parts.

[0021] Wherein, the preparation method of the modified nano iris is: put 70 parts by weight of the nano iris into a 25% glacial acetic acid solution and soak for 4 hours, take it out and rinse until it is neutral, and dry it to moisture content at 55°C It is 4%; add 5 parts of castor oil and mix evenly, then add 4 parts of dimercaptopropanol and 2 parts of nano graphite powder, mix and grind, and pass through a 200-mesh sieve.

[0022] Preparation method of ceramic composite material:

[0023] Step S1, ball-milling nano-titanium carbide, nano-titanium nitride, nano-silicon carbide, calcite powder and modified nano-iris c...

Embodiment 2

[0026] Example 2: Preparation of ceramic composite materials

[0027] Weight ratio of raw materials: nano titanium carbide, 35 parts; nano titanium nitride, 30 parts; nano silicon carbide, 25 parts; calcite powder, 5 parts; modified nano illite, 5 parts; deionized water, 8 parts; minerals Oil, 6 parts; Silane coupling agent KH560, 3 parts; Fumaric acid, 2 parts.

[0028] Wherein, the preparation method of the modified nano iris is: put 70 parts by weight of the nano iris into a 25% glacial acetic acid solution and soak for 4 hours, take it out and rinse until it is neutral, and dry it to moisture content at 55°C It is 4%; add 5 parts of castor oil and mix evenly, then add 4 parts of dimercaptopropanol and 2 parts of nano graphite powder, mix and grind, and pass through a 200-mesh sieve.

[0029] Preparation method of ceramic composite material:

[0030] Step S1, ball-milling nano-titanium carbide, nano-titanium nitride, nano-silicon carbide, calcite powder and modified nano-iris clay...

Embodiment 3

[0033] Example 3: Preparation of ceramic composite materials

[0034] Weight ratio of raw materials: nano titanium carbide, 45 parts; nano titanium nitride, 40 parts; nano silicon carbide, 35 parts; calcite powder, 15 parts; modified nano iris clay, 15 parts; deionized water, 12 parts; minerals Oil, 10 parts; Silane coupling agent KH560, 5 parts; Fumaric acid, 4 parts.

[0035] Wherein, the preparation method of the modified nano iris is: put 70 parts by weight of the nano iris into a 25% glacial acetic acid solution and soak for 4 hours, take it out and rinse until it is neutral, and dry it to moisture content at 55°C It is 4%; add 5 parts of castor oil and mix evenly, then add 4 parts of dimercaptopropanol and 2 parts of nano graphite powder, mix and grind, and pass through a 200-mesh sieve.

[0036] Preparation method of ceramic composite material:

[0037] Step S1, ball-milling nano-titanium carbide, nano-titanium nitride, nano-silicon carbide, calcite powder and modified nano-ir...

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PUM

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Abstract

The invention discloses a high-strength and high-toughness ceramic composite and preparation thereof. The ceramic composite is prepared from raw materials in parts by weight as follows; 35-45 parts of nano titanium carbide, 30-40 parts of nano titanium nitride, 25-35 parts of nano silicon carbide, 5-15 parts of calcite powder, 5-15 parts of modified nano illite, 8-12 parts of deionized water, 6-10 parts of mineral oil, 3-5 parts of a saline coupling agent KH560 and 2-4 parts of fumaric acid; a preparation method of the modified nano illite comprises steps as follows: 60-80 parts of nano illite by weight are placed in a glacial acetic acid solution with the mass fraction being 20%-30% to be soaked for 3-5 h, taken out, washed to be neutral and dried at 50-60 DEG C until the moisture content is 3%-5%; 4-6 parts of castor oil are added and evenly mixed, 3-5 parts of dimercaprol and 1-3 parts of nano graphite powder are added, mixing and grinding are performed, and the mixture is sieved by a 200-mesh sieve, and the ceramic composite is prepared. The ceramic composite has high hardness, strength and toughness, and the preparation method is simple.

Description

Technical field [0001] The invention belongs to the field of materials, and specifically relates to a high-strength, high-toughness ceramic composite material and preparation thereof. Background technique [0002] Composite materials usually have good comprehensive properties in which different materials complement each other's strengths. Composite materials have the characteristics of two or more materials and can improve the performance of a single material, such as increasing strength, increasing toughness, and improving dielectric properties. Ceramic composite materials used as high-temperature structural materials are mainly used in aerospace, military and other sectors. In addition, various ceramic composite materials are widely used in the fields of machinery, chemical industry, and electronic technology. [0003] Ceramic matrix composite material is a kind of composite material that is composited with various fibers with ceramic as the matrix. The ceramic substrate can b...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/56C04B35/622
CPCC04B35/5611C04B35/622C04B2235/3208C04B2235/349C04B2235/3826C04B2235/3886C04B2235/5454C04B2235/96
Inventor 谢超
Owner 江西新宏信陶瓷有限公司
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