Organosilicon waterproof dustproof anticorrosion adhesive, and preparation method and application thereof
A technology of three-proof glue and silicone, which is applied in the direction of adhesives, adhesive additives, non-polymer adhesive additives, etc., can solve the problems of poor waterproof effect, high cost and complicated preparation process of small-pitch high-definition display screens, and achieve Improvement of working stability and reliability, reduction of viscosity, and expansion of application range
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Embodiment 1
[0027] Preparation of synthetic reinforcing agent: mix ethyl orthosilicate, polymethyltriethoxysilane, trimethylsilanol, ethanol, and acetic acid aqueous solution in a weight ratio of 100:30:150:60:5, and heat at 40°C Under the conditions of reaction for 3 hours, then under the conditions of 30 ℃ and pressure -0.5MPa, low molecular solvents such as ethanol, methanol and water were distilled off to obtain an oily viscous and transparent synthetic reinforcing agent.
[0028] Preparation of silicone conformal adhesive: component A is mixed with hydroxyl-terminated polydimethylsiloxane, dimethyl silicone oil, synthetic reinforcing agent and diluent in a weight ratio of 100:20:10:60, packaged ; Component B is formed by mixing crosslinking agent, catalyst, coupling agent and diluent in a weight ratio of 6.0:5.0:10:180, and packaged. A component and B component are mixed in a weight ratio of 1:1.
[0029] Mix component A and component B and stir evenly, pour into the mold, the surfa...
Embodiment 2
[0031] Preparation of synthetic reinforcing agent: Mix ethyl orthosilicate, polymethyltriethoxysilane, trimethylsilanol, ethanol, and acetic acid aqueous solution in a weight ratio of 100:30:200:60:5, and heat at 60°C Under the conditions of reaction for 4 hours, then under the conditions of 50 ℃ and pressure -0.1MPa, low molecular solvents such as ethanol, methanol and water were distilled off to obtain an oily viscous and transparent synthetic reinforcing agent.
[0032] Preparation of silicone conformal adhesive: component A is mixed with hydroxyl-terminated polydimethylsiloxane, dimethyl silicone oil, synthetic reinforcing agent and diluent in a weight ratio of 100:20:20:60, packaged ; Component B is made by mixing cross-linking agent, catalyst, coupling agent and diluent in a weight ratio of 6:4.0:8:160, and packaged. A component and B component are mixed in a weight ratio of 1:1.
[0033] Mix component A and component B and stir evenly, pour into the mold, the surface d...
Embodiment 3
[0035] Preparation of synthetic reinforcing agent: mix ethyl orthosilicate, polymethyltriethoxysilane, trimethylsilanol, ethanol, and acetic acid aqueous solution in a weight ratio of 100:50:200:60:10, and heat at 45°C Under the conditions of reaction for 4 hours, then under the conditions of 40 ℃ and pressure -0.3MPa, low molecular solvents such as ethanol, methanol and water were distilled off to obtain an oily viscous and transparent synthetic reinforcing agent.
[0036] Preparation of silicone conformal adhesive: component A is mixed with hydroxyl-terminated polydimethylsiloxane, dimethyl silicone oil, synthetic reinforcing agent and diluent in a weight ratio of 100:30:20:80, packaged ; Component B is formed by mixing cross-linking agent, catalyst, coupling agent and diluent in a weight ratio of 10:2.0:12:150, and packaged. A component and B component are mixed in a weight ratio of 1:1.
[0037] Mix component A and component B and stir evenly, pour into the mold, the surf...
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