Application of terephthalic acid-europium fluorescent probe containing 1-ethyl-3-methylimidazole in aniline detection
A technology of terephthalic acid and methylimidazole, applied in the application field of terephthalic acid-europium fluorescent probe in the detection of aniline, can solve the problems of slow reaction, complicated operation and high cost, and achieve high selectivity and high Sensitivity, good recyclability effect
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[0019] 0.1836g (0.5mmol) EuCl 3 ·6H 2 O, 0.0832g (0.5mmol) terephthalic acid and 0.8006g (5.5mmol) chloride 1-ethyl-3-methylimidazolium ionic liquid are added in the reactor of 25mL polytetrafluoroethylene liner, mix well, then Place the reaction kettle in an oven, react at 170°C for 5 days, cool to room temperature, and wash with acetone and ethanol to obtain a colorless and transparent block of terephthalic acid containing 1-ethyl-3-methylimidazole- Europium fluorescent probes such as figure 1 As shown, its structural unit is [EMI] 2 [Eu 2 (BDC) 3 (H 2 -BDC)Cl 2 ], where EMI represents 1-ethyl-3-methylimidazole, H 2 -BDC means terephthalic acid, BDC means terephthalate that has lost protons on two carboxyl groups, belongs to the monoclinic crystal system, and the space group is P 2 1 / n, the unit cell parameter is β=104.088(3)°, unit cell volume Z=4.
[0020] 1. Fluorescence performance test
[0021] The inventor used the solid-state fluorescence test method ...
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