A kind of red pigment for zirconia ceramics, its preparation method and its application
A technology of zirconia ceramics and a production method, which is applied in the direction of fibrous fillers, etc., can solve the problems of dull color and uneven coloring of ceramics, and achieve the effects of bright red, good color rendering effect, and good color rendering effect
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Embodiment 1
[0107] A red colorant for zirconia ceramics, the red colorant in this embodiment only includes a color-developing substance, and the color-developing substance is a powder prepared by compounding according to the following formula:
[0108] xABO 3 +yR 2 O 3 +zC
[0109] Among them, A represents Ba, B represents Ti, and R represents rare earth elements Sm and Y. In the formula of this example, Sm 2 O 3 and Y 2 O 3 The mass ratio of 1:1, C represents MnO 2 ;
[0110] Wherein, x=0.5mol; y=0.04mol; z=0.2mol.
[0111] The red colorant preparation method of the present embodiment is as follows:
[0112] The pretreatment is to remove impurities from the oxide raw material used to make the color-developing substance, and then calcinate after the removal of impurities. After the calcination is completed, it is ground with a mortar. Specifically, the calcination temperature is 600°C, and the calcination time is 1h;
[0113] Batching, ball milling, mixing and drying, the pretre...
Embodiment 2-9
[0116] The red colorant of Examples 2-9 of the present application also only includes color-developing substances, and is roughly the same as the formula and preparation method of the red colorant in Example 1, except that A, B, R, C, The selection and values of x, y, and z are slightly different from those in Example 1, and the specific parameters in the production method are different.
[0117] Wherein, the specific difference of ingredient molecular formula is as follows:
[0118] Table 1
[0119]
[0120] In Table 1, the molar ratio of Sn and Se in Example 2 is 2:1, the molar ratio of Y and La is 1:3, MnO 2 with Al 2 O 3 The molar ratio is 1:1;
[0121] In Table 1, the molar ratio of Mg, Ca and Ba in Example 3 is 1:2:1, the molar ratio of Ho and Dy is 2:3, Cr 2 O 3 with CaF 2 The molar ratio is 1:1;
[0122] In Table 1, the mol ratio of Er and Nd in Example 5 is 1:5;
[0123] In Table 1, the molar ratio of Zn to Sr in Example 6 is 2:1, the molar ratio of Ti t...
Embodiment 10
[0148] A red colorant for zirconia ceramics. The difference between this embodiment and Examples 1-9 is that the red colorant in this embodiment not only includes a color-developing substance, but also includes a high-temperature phase package coated on the surface of the color-developing substance. Coating layer. Correspondingly, in a method for manufacturing a red color material for zirconia ceramics in this embodiment, a heterogeneous coating technology is used to coat the high-temperature phase coating layer on the surface of the color-developing substance.
[0149] Specifically, the present embodiment adopts the color-developing substance of Example 1 to further produce the red colorant by using the heterogeneous wrapping technology, and the heterogeneous wrapping technology specifically includes the following steps:
[0150] Addition of amphoteric surfactant: add the color-developing substance to the aqueous solution containing the amphoteric surfactant, stir to combine t...
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