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A kind of surface treatment method of medical degradable metal interventional stent

A surface treatment and metal technology, which is applied in the field of surface treatment of medical degradable metal interventional stents, can solve the problems of complex phosphoric acid and polyol system, less electropolishing of degradable metals, poor repeatability and stability, etc., and achieves repeatable operation. High performance, good surface quality, easy to formulate effect

Active Publication Date: 2018-09-28
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For hollow stents with complex patterns, mechanical polishing in the traditional sense is difficult to operate and has low efficiency. Currently, vascular stents in clinical use are all electropolished.
But there is less electrolytic polishing for degradable metals, especially in the medical field
A small number of studies use perchloric acid-absolute ethanol solution as the electrolytic polishing solution, which is prone to explosion
However, the phosphoric acid and polyol system is complicated, which makes the preparation of the electrolyte difficult, and the repeatability and stability are poor.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] The degradable metal interventional stent to be processed in this embodiment is specifically a degradable magnesium interventional stent. In this embodiment, the surface treatment method of the degradable metal intervention stent comprises the following steps:

[0028] Step 1. Sandblasting the degradable metal interventional bracket. The specific sandblasting process is: sandblasting pressure 0.1MPa, sandblasting angle 20°, sandblasting distance 6cm, sandblasting time 10s;

[0029] Step 2. The degradable metal interventional stent after sandblasting in step 1 is immersed in metal cleaning agent, deionized water and absolute ethanol in order to perform the first ultrasonic cleaning treatment, and the degradable metal interventional stent is cleaned in metal cleaning agent, The time for the first ultrasonic cleaning treatment in deionized water and absolute ethanol is both 15 minutes, and the temperature is 40° C., and then the degradable metal interventional stent after ...

Embodiment 2

[0035] The degradable metal interventional stent to be processed in this embodiment is specifically a degradable zinc interventional stent. In this embodiment, the surface treatment method of the degradable metal intervention stent comprises the following steps:

[0036] Step 1. Sandblasting the degradable metal interventional bracket. The specific sandblasting process is: sandblasting pressure 0.15MPa, sandblasting angle 40°, sandblasting distance 8cm, sandblasting time 40s;

[0037] Step 2. The degradable metal interventional stent after sandblasting in step 1 is immersed in metal cleaning agent, deionized water and absolute ethanol in order to perform the first ultrasonic cleaning treatment, and the degradable metal interventional stent is cleaned in metal cleaning agent, The time for the first ultrasonic cleaning treatment in deionized water and absolute ethanol is both 20 minutes, and the temperature is 40° C., and then the degradable metal interventional stent after the ...

Embodiment 3

[0043] The degradable metal interventional stent to be processed in this embodiment is specifically a degradable magnesium alloy AZ31 interventional stent. In this embodiment, the surface treatment method of the degradable metal intervention stent comprises the following steps:

[0044] Step 1. Sandblasting the degradable metal interventional bracket. The specific sandblasting process is: sandblasting pressure 0.2MPa, sandblasting angle 60°, sandblasting distance 10cm, sandblasting time 60s;

[0045] Step 2. The degradable metal interventional stent after sandblasting in step 1 is immersed in metal cleaning agent, deionized water and absolute ethanol in order to perform the first ultrasonic cleaning treatment, and the degradable metal interventional stent is cleaned in metal cleaning agent, The time for the first ultrasonic cleaning treatment in deionized water and absolute ethanol is both 25 minutes, and the temperature is 40° C., and then the degradable metal interventional ...

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PUM

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Abstract

The invention provides a surface treatment method for a degradable metal intervention stent, comprising the following steps: 1. performing sandblasting on the degradable metal intervention stent; 1. Ultrasonic cleaning treatment, and then vacuum drying; 3. Electrolytic polishing; 4. Submerging in deionized water and absolute ethanol for the second ultrasonic cleaning treatment, and then vacuum drying; 5. Passivation. The degradable metal interventional stent treated by the invention has good surface quality and high smoothness, can be placed in the atmosphere for a long time, and the corrosion resistance is significantly improved.

Description

technical field [0001] The invention belongs to the technical field of surface treatment of medical metal materials, and in particular relates to a surface treatment method of a medical degradable metal interventional bracket. Background technique [0002] For a long time, cardiovascular and cerebrovascular diseases have been the number one killer threatening human health. With the development of endovascular treatment technology, endovascular stent implantation has become one of the most effective methods for the treatment of cardiovascular diseases. Stent materials commonly used in early clinical applications include stainless steel, titanium and titanium alloys, and Co-Cr alloys. Although these materials can exist in the human body for a long time as foreign bodies, they will cause excessive proliferation of the vascular intima and cause restenosis of the vascular wall, eventually leading to implant failure. [0003] In recent years, degradable metal scaffold materials ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C25F3/18C23C22/68B24C1/00
CPCB24C1/00C23C22/68C25F3/18C25F3/22
Inventor 于振涛余森王昌牛金龙张彪
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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