A lithium ion battery negative electrode material fe2sis4 and its composite material fe2sis4/cpan
A technology for lithium-ion batteries and negative electrode materials, applied in battery electrodes, secondary batteries, circuits, etc., can solve the problems of complex preparation methods and difficulty in large-scale production, and achieve simple and easy-to-operate synthesis methods, easy popularization and application, and wide sources Effect
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[0020] Weigh Fe, Si, S with a total mass of 240mg (Fe / Si / S molar ratio is 2:1:4). Weigh 60mg of PAN, fully grind to a finer powder. Add the weighed medicine to the ground PAN powder, and grind until mixed evenly. After the raw materials are pressed into tablets, they are vacuum-sealed into a quartz tube and transferred to a muffle furnace for temperature control. The temperature was raised from room temperature to 300° C. over 10 hours and kept at that temperature for 10 hours. Then, after 10 hours, the temperature was raised to 800-1000°C, and the temperature was kept for 24 hours, and then the program was stopped. After cooling to room temperature, open the quartz tube to take out the product, and grind it for later use. Pure Fe 2 SiS 4 Same operation as above. Product Features:
[0021] figure 1 Is the embodiment solid phase reaction product Fe 2 SiS 4 and Fe 2 SiS 4 XRD pattern of / CPAN. The reaction gives Fe 2 SiS 4 and Fe 2 SiS 4 / XRD pattern of CPAN and...
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