Phase change energy storage powder for building energy saving and preparation method thereof
A phase-change energy storage and building energy-saving technology, which is applied in the direction of chemical instruments and methods, heat exchange materials, etc., can solve the performance degradation of building materials, the reduction of energy storage density of phase-change composite materials, and unsatisfactory compatibility, etc. problems, to achieve the effect of solving leakage and broadening the scope of adaptation
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Embodiment 1
[0039] (1) Surface modification of phase change materials: 40 parts by weight of calcium chloride hexahydrate, 45 parts by weight of sodium sulfate decahydrate phase change materials, 0.1 parts by weight of sodium metaaluminate, 2 parts by weight of glycerin fatty acid The ester is refined into a powder with a particle size of less than 2 μm to obtain a modified phase change material;
[0040] (2) Extrusion coating: Mix the modified phase change material obtained in step (1) with 12 parts by weight of ethylene-vinyl acetate copolymer, 2 parts by weight of aluminum powder, and 0.5 parts by weight of antioxidant 1010 at high speed Disperse evenly in the machine, and then send it to the screw extruder. The temperature setting method of the screw extruder is: 50°C~60°C for the first to third zones; 6°C~80°C for the fourth to sixth zones; 50°C~60°C for the seventh to ninth zones The tenth zone is 40°C; the screw speed is 50~100r / min; the material enters from the first zone and is e...
Embodiment 2
[0044] (1) Surface modification of phase change materials: 50 parts by weight of disodium hydrogen phosphate dodecahydrate, 30 parts by weight of sodium acetate trihydrate, 0.2 parts by weight of sodium borate anti-supercooling agent, 3 parts by weight of titanic acid The ester couple is refined into a powder with a particle size of less than 2 μm to obtain a modified phase change material;
[0045] (2) Extrusion coating: Mix the modified phase change material obtained in step (1) with 10 parts by weight of polypropylene wax, 1 part by weight of graphite powder as a heat-conducting agent, and 0.8 parts by weight of barium laurate stabilizer at high speed Disperse evenly in the machine, and then send it into the twin-screw extruder. The temperature setting method of the screw extruder is: 50℃~60℃ for the first to third zones; 6℃~80℃ for the fourth to sixth zones; 50℃~ for the seventh to ninth zones 60°C; 40°C in the tenth zone; the screw speed is 50~100r / min; the material enter...
Embodiment 3
[0049] (1) Surface modification of phase change materials: 35 parts by weight of sodium sulfate decahydrate, 45 parts by weight of sodium acetate trihydrate, 0.3 parts by weight of anti-supercooling agent potassium pyroantimonate, 2 parts by weight of polyoxyethylene Fatty acid glycerides are refined into powders with a particle size of less than 2 μm to obtain modified phase change materials;
[0050] (2) Extrusion coating: the modified phase change material obtained in step (1) is mixed with 8 parts by weight of rosin, 2 parts by weight of copper powder of thermal conductivity agent, and 0.6 parts by weight of stabilizer and antioxidant DLTP in a high-speed mixer Evenly dispersed in the medium, and then sent to the screw extruder, the temperature setting method of the screw extruder is: 50°C~60°C for the first to third zones; 6°C~80°C for the fourth to sixth zones; 50°C~60°C for the seventh to ninth zones; The tenth zone is 40°C; the screw speed is 50~100r / min; the material ...
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