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Staining solution for zirconia ceramic for dental department

A zirconia ceramic and dyeing solution technology, applied in dentures and other directions, can solve the problems of complex process, increased PE film printing and coloring and heat treatment, less penetration and coloring technology for all-ceramic teeth, etc. The effect of preventing blind dyeing

Inactive Publication Date: 2016-09-28
CHENGDU BESMILE BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this method increases the preparation of PE film, printing and coloring and heat treatment, making the whole process quite complicated.
At the same time, literature searches at home and abroad show that there are very few research reports on the infiltration coloring technology of all-ceramic teeth.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Embodiment 1: a kind of staining solution for dental zirconia ceramics, it is made up of the raw material of following concentration:

[0023] Colorant: 0.5mol / L; Dispersant: 7.5wt%;

[0024] Complexing agent: 0.1mol / L; Thixotropic agent: 6.5wt%;

[0025] Color indicator: 0.2 wt%.

[0026] The coloring agent includes coloring cations and coloring anions, wherein the coloring cations are iron ions and erbium ions; the coloring solution anions are chloride ions; the dispersant is stearic acid; the complexing agent is formic acid; The color indicator is methyl violet; the thixotropic agent is a hydroxyethyl cellulose derivative.

Embodiment 2

[0027] Embodiment 2: a kind of staining solution for dental zirconia ceramics, it is made up of the raw material of following concentration:

[0028] Colorant: 0.004mol / L; Dispersant: 2wt%;

[0029] Complexing agent: 0.002mol / L; Thixotropic agent: 3wt%;

[0030] Color indicator: 0.05wt%.

[0031] The coloring agent includes a coloring cation and a coloring anion, wherein the coloring cation is a combination of praseodymium ion, manganese ion and cobalt ion; the coloring liquid anion is nitrate and permanganate; the dispersant is dodecane The combination of sodium base sulfate and methyl amyl alcohol; the complexing agent is the combination of acetic acid and oxalic acid; the color indicator is the combination of malachite green and bromophenol blue sodium; the thixotropic agent is polyvinyl alcohol and polyvinyl alcohol Combination of amide waxes.

Embodiment 3

[0032] Embodiment 3: a kind of staining solution for dental zirconia ceramics, it is made up of the raw material of following concentration:

[0033] Colorant: 1mol / L; Dispersant: 13wt%;

[0034] Complexing agent: 0.2mol / L; Thixotropic agent: 10wt%;

[0035] Color indicator: 0.4 wt%.

[0036] The coloring agent includes coloring cations and coloring anions, wherein the coloring cations are a combination of manganese ions, cobalt ions and zinc ions; the coloring solution anion is a combination of permanganate, sulfate and acetate; The agent is a combination of cellulose derivatives, polyacrylamide and gull gum; the complexing agent is a combination of succinic acid, adipic acid and benzoic acid; the color indicator is methyl orange, sodium bromothymol blue and the combination of methyl yellow; the thixotropic agent is the combination of hydrogen polyvinyl alcohol, polyamide wax and polydextrose.

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PUM

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Abstract

The invention discloses a staining solution for zirconia ceramic for the dental department. The staining solution is composed of a coloring agent, a dispersing agent, a complexing agent, a thixotropic agent and a color indicator. According to the staining solution, the color indicator is added, so that the staining solution can show different colors before sintering; and the dyeing time can be adjusted according to the color shade, so that the blind dyeing can be prevented. With the adoption of the staining solution, the defects that the penetration coloring technology is limited by human factors, and the penetration coloring process of the all-ceramic crown has the blindness and the experimental property are overcome, and the staining solution has the advantages that the dyeing penetration time is short, the stability is strong, and the all-ceramic crown product is high in high-quality rate; the staining solution is simple in production and using method, easily available in raw materials, low in cost, and suitable for large-scale industrial production.

Description

technical field [0001] The invention relates to the technical field of material science, in particular to a dyeing solution for dental zirconia ceramics. Background technique [0002] At present, the technology of making all-ceramic restorations with dental CAD / CAM technology is quite mature, which can fully realize the automatic processing and the production of high-strength all-ceramic crowns and bridges. As the most important dental all-ceramic crown material, zirconia is characterized by its white to ivory color after sintering. Although it has a certain degree of translucency, it cannot meet the clinical requirements for the color of the restoration. In order to meet the color requirements of clinical dentures, it is often necessary to shade the all-ceramic base crown to lose part of its transparency. By adjusting the transparency, color and saturation of zirconia itself, it is consistent with the tooth to be restored. The denture after staining can save the preparatio...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61C13/083
CPCA61C13/083
Inventor 易元超
Owner CHENGDU BESMILE BIOTECH
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