Thixotropic epoxy resin, preparation method and application in LED chip packaging
A technology of epoxy resin and aliphatic epoxy resin, applied in epoxy resin glue, adhesive type, semiconductor devices, etc., can solve the problems of unsuitable chips and LED displays, high residual stress, low production efficiency, etc. , to avoid mixing and dispensing process, easy control of process parameters, and improve production efficiency
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Embodiment 2
[0043] The mixing temperature of Example 2 is the same as that of Example 1.
[0044] The components of Example 3 were mixed uniformly at a temperature of 35° C. to obtain mixture 1 of Example 3.
Embodiment 4
[0045] The mixing temperature of Example 4 is the same as that of Example 3.
[0046] The components of Example 5 were mixed uniformly at a temperature of 50° C. to obtain Mixture 1 of Example 5.
[0047] The mixing temperature of Example 6, 7 or 8 is the same as that of Example 5.
[0048] Experiments have proved that 0.05 parts by weight of 2,4,6 tris[2-(3,4-epoxycyclohexylethyl)]tetramethylcyclotetrasiloxane, bis[2-(3,4 -Epoxycyclohexylethyl)]tetramethylcyclotetrasiloxane, 2,4,6,8-tetramethyl-[2-(3,4-epoxycyclohexylethyl)]cyclotetrasiloxane Alkyl, 2,4,6,8-tetramethyl-2,4,6,8-tetra[3-(oxiranylmethoxy)propyl]cyclotetrasiloxane, 2,4,6 ,8-Tetramethyl-2-[3-(oxiranylmethoxy)propyl]cyclotetrasiloxane replaces 0.05 parts of γ-methacryloxypropyltrimethoxy in Example 1 The other silanes are the same as in Example 1, and the mixture is uniformly mixed at a temperature of 25°C. The obtained mixture one can be used to prepare a thixotropic epoxy resin.
[0049] Experiments have shown that 0....
Embodiment 10
[0053] The reaction temperature and reaction time of Example 10 are the same as those of Example 9.
[0054] The components of Example 11 were reacted for 2 hours at a temperature of 100° C. to obtain the second mixture of Example 11;
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