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Antibacterial viscose and preparation method thereof

A viscose fiber and berberine technology, applied in the textile field, can solve problems such as unfavorable human health, loss of antibacterial effect, uncomfortable close-fitting clothing, etc., and achieve the effect of maintaining excellent characteristics for a long time, improving taking performance, and good antibacterial effect.

Active Publication Date: 2016-08-31
汕头市珂玲服饰有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Most of the existing antibacterial fabrics are chemically synthesized fabrics, which are not comfortable enough to be used as close-fitting clothing; there are also built-in silver ion antibacterial fabrics, which use spinning-grade antibacterial technology to directly put antibacterial agents into chemical fibers , but silver ions have strong neurotoxicity, which is not conducive to human health; there are also fabrics soaked in traditional Chinese medicine liquid, but this fabric is not washable, and it loses its antibacterial effect after being washed many times; in addition, some fibers It has certain antibacterial properties, but the antibacterial spectrum is small, and it is only inhibitory to a few types of bacteria. There are many types of bacteria in contact with it in life, and it can still infect bacteria

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Antibacterial viscose and preparation method thereof
  • Antibacterial viscose and preparation method thereof
  • Antibacterial viscose and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Prepare antibacterial viscose fiber 1, following steps:

[0032] Step 1: Grind 5 kg of Coptidis rhizoma into powder, add 30 kg of aqueous ethanol solution with a mass fraction of 55%, conduct ultrasonic extraction for 1.5 hours at a temperature of 80°C, the ultrasonic frequency is 28KHZ, filter and take the filtrate to obtain the berberine extract, adjust with hydrochloric acid pH = 2, stirred, cooled to 8°C, left to stand for 20 hours, filtered to obtain crystals, recrystallized with water, filtered to obtain berberine, dried in a 50°C oven to obtain 38g of berberine, prepared from berberine Ultrafine powder with powder particles less than 5μm;

[0033] Step 2, weighing chitin and sodium alginate, respectively preparing ultrafine powders with powder particles less than 5 μm;

[0034] Step 3. Preparation of cotton linter viscose fiber spinning stock solution in the aging process: specifically, soluble cellulose sulfonic acid is prepared by cooking, soaking, pressing, p...

Embodiment 2

[0041] Prepare antibacterial viscose fiber 2, following steps:

[0042] Step 1: Grind 5 kg of Coptis Rhizoma into powder, add 35 kg of aqueous ethanol solution with a mass fraction of 40%, conduct ultrasonic extraction at a temperature of 70°C for 1 hour, and the ultrasonic frequency is 30KHZ, filter and take the filtrate to obtain the berberine extract, adjust with hydrochloric acid pH=1, stir, cool down to 0°C, let stand for 16 hours, filter to obtain crystals, recrystallize with water, filter to obtain berberine, place in a 60°C drying oven to dry, and obtain 19.3g of berberine. Prepare ultrafine powder with powder particles less than 5 μm;

[0043] Step 2, weighing chitin and sodium alginate, respectively preparing ultrafine powders with powder particles less than 5 μm;

[0044] Step 3. Preparation of cotton linter viscose fiber spinning stock solution in the aging process: specifically, soluble cellulose sulfonic acid is prepared by cooking, soaking, pressing, pulverizing,...

Embodiment 3

[0051] Prepare antibacterial viscose fiber 1, following steps:

[0052] Step 1: Grind 5 kg of Coptis Rhizoma into powder, add 40 kg of aqueous ethanol solution with a mass fraction of 70%, conduct ultrasonic extraction at a temperature of 75° C. for 2 hours, the ultrasonic frequency is 40 KHZ, filter the filtrate to obtain a berberine extract, adjust with hydrochloric acid pH=2, stirring, cooling to 10°C, standing for 14 hours, filtering to obtain crystals, recrystallizing with water, filtering to obtain berberine, and drying in a 50°C oven to obtain 21.6g of berberine. Prepare ultrafine powder with powder particles less than 5 μm;

[0053] Step 2, weighing chitin and sodium alginate, respectively preparing ultrafine powders with powder particles less than 5 μm;

[0054] Step 3. Preparation of cotton linter viscose fiber spinning stock solution in the aging process: specifically, soluble cellulose sulfonic acid is prepared by cooking, soaking, pressing, pulverizing, aging, ye...

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Abstract

The invention discloses antibacterial viscose and a preparation method thereof, belonging to the technical field of textiles. The viscose is prepared by mixing berberine, sodium alginate, chitin and a viscose spinning solution and then spinning the mixture. The prepared antibacterial viscose is prepared by blending the natural extracts including berberine, chitin and sodium alginate, and the spinning solution, is comfort to wear, can effectively prevent plaques and odors on clothes and promote wound healing, is safe and nontoxic, has good hygienic property, is harmless to human bodies after being worn for a long term and is extremely suitable for manufacturing medical nurse uniforms, supplies for rescue, such as bandage gauzes, bedding, such as bed sheets and quilt covers, healthcare baby clothes and underclothes.

Description

technical field [0001] The invention belongs to the technical field of textiles, and more specifically relates to an antibacterial viscose fiber and a preparation method thereof. Background technique [0002] Viscose fiber is a cellulose fiber produced from cotton or other natural fibers. Among the 12 main textile fibers, the moisture content of viscose fiber is most in line with the physiological requirements of human skin, and it has the characteristics of smooth and cool, breathable, antistatic, and brilliant dyeing. As one of the three raw materials for spinning (cotton, polyester, viscose), viscose fiber has the advantages of both cotton and polyester: its moisture absorption, anti-electricity and softness are superior to polyester, and its drapability and dyeability are superior to polyester. Cotton fiber. [0003] Berberine is a common isoquinoline alkaloid with the molecular formula [C20H18NO4]+. It is a long-used traditional Chinese medicine in my country and can ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F2/08
CPCD01F2/08
Inventor 胡稳成
Owner 汕头市珂玲服饰有限公司
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