Preparation method for boron carbonitride nanosheet loaded metal nano particle hybrid material
A technology for loading metals and nanoparticles, which is applied in the field of nanomaterials and achieves the effects of good application prospects, simple synthesis process and short cycle.
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Embodiment 1
[0019] Preparation of boron-carbon-nitrogen nanosheet-supported metal nickel nanoparticle hybrid material :
[0020] Add 200 mg of nickel nitrate, 200 mg of glycine and 50 mg of boric acid into a beaker, disperse in 5 mL of deionized water, and transfer the resulting mixture to an alumina porcelain boat after ultrasonication for 0.5 hours; place the above alumina porcelain boat in a tube After raising the temperature in the furnace to 400° C. and keeping it warm for 1 hour, and then cooling naturally, a boron carbon nitrogen nanosheet-loaded metal nickel nanoparticle hybrid material was obtained.
Embodiment 2
[0022] Preparation of boron-carbon-nitrogen nanosheet-supported metal nickel nanoparticle hybrid material :
[0023] Add 200 mg of nickel nitrate, 50 mg of glycine and 50 mg of boric acid into a beaker, disperse in 5 mL of deionized water, and transfer the resulting mixture to an alumina porcelain boat after ultrasonication for 0.6 hours; place the above alumina porcelain boat in a tube The furnace was heated to 500 ° C and kept for 3 hours, and then cooled naturally to obtain a boron carbon nitrogen nanosheet-supported metal nickel nanoparticle hybrid material.
Embodiment 3
[0025] Preparation of boron-carbon-nitrogen nanosheet-supported metal nickel nanoparticle hybrid material :
[0026] Add 200 mg of nickel nitrate, 600 mg of glycine and 60 mg of boric acid into a beaker, disperse in 5 mL of deionized water, and transfer the resulting mixture to an alumina porcelain boat after ultrasonication for 1 hour; place the above alumina porcelain boat in a tube The furnace was heated to 800 ° C and kept for 5 hours, and then cooled naturally to obtain a boron carbon nitrogen nanosheet-supported metal nickel nanoparticle hybrid material.
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