Method for manufacturing large-specification carbon graphite sealing material matrix
A technology of sealing materials and carbon graphite, which is applied in the field of preparation of large-scale carbon graphite sealing material substrates, can solve the problems of not meeting the specifications of large-scale equipment sealing devices, product specifications cannot be enlarged, and the process is complicated, so as to reduce the number of carbonization, Effect of increasing density and reducing porosity
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Embodiment 1
[0030] A kind of embodiment of the preparation method of large-scale carbon graphite sealing material matrix of the present invention, comprises the following steps:
[0031] (1) Preparation of secondary carbon black powder and modified asphalt slurry
[0032] The carbon black was pulverized by air flow until the particle size (D50) was 5 μm to 6 μm, then 30 kg of carbon black powder was fed into the vacuum kneader, and the cover was opened and mixed at 170 ° C for 1 h, and the modified bitumen in a molten state of 185 ° C (softening point 115°C) 12kg, close the machine cover, control the temperature at 190°C, control the positive speed of the kneader at 30r / min, vacuumize and knead for 2 hours, and put the paste out of the pot after kneading into the machine while it is hot. Make it into a cylindrical shape at not lower than 150°C, then raise the temperature for carbonization (the highest temperature reaches 1100°C), cool to room temperature after carbonization, and obtain se...
Embodiment 2
[0041] A kind of embodiment of the preparation method of large-scale carbon graphite sealing material matrix of the present invention, comprises the following steps:
[0042] (1) Preparation of secondary carbon black powder and modified asphalt slurry
[0043] The carbon black was pulverized by air flow until the particle size (D50) was 5 μm to 6 μm, and then 30 kg of carbon black powder was fed into the vacuum kneader, and the lid was opened and mixed at 150 ° C for 1 h, and the modified pitch (softening point (115°C) 10kg, close the machine cover, control the temperature at 175°C, control the reverse speed of the kneader at 20r / min, vacuumize and knead for 2 hours, and put the paste out of the pot after kneading into the machine while it is hot. Make it into a cylinder at a temperature not lower than 150°C, then raise the temperature for carbonization (the maximum temperature reaches 1000°C), cool to room temperature after carbonization, and obtain secondary carbon black pow...
Embodiment 3
[0052] A kind of embodiment of the preparation method of large-scale carbon graphite sealing material matrix of the present invention, comprises the following steps:
[0053] (1) Preparation of secondary carbon black powder and modified asphalt slurry
[0054] The carbon black was pulverized by air flow until the particle size (D50) was 5 μm to 6 μm, and then 30 kg of carbon black powder was fed into the vacuum kneader, and the lid was opened and mixed at 160 ° C for 1 h, and the modified asphalt (softening point 115°C) 15kg, close the machine cover, control the temperature at 200°C, control the forward and reverse rotation speed of the kneader at 25r / min, vacuumize and knead for 2 hours, put the paste out of the pot after kneading into the machine while it is hot, and Turn it into a cylinder at a temperature not lower than 160°C, then raise the temperature for carbonization (the maximum temperature reaches 1150°C), cool to room temperature after carbonization, and obtain seco...
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