Preparation method for ferrite, ferrite and inductor
A technology of ferrite and nickel oxide, applied in the direction of transformer/inductor core, etc., can solve the problem of ferrite's weak resistance to current impact
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[0024] The preparation method of ferrite will be further described in detail mainly in conjunction with the accompanying drawings.
[0025] Such as figure 1 As shown, the method for preparing ferrite according to one embodiment includes the following steps S110-S160.
[0026] S110, providing pre-fired ingredients, the pre-fired ingredients include iron oxide, nickel oxide, zinc oxide, copper oxide and tricobalt tetroxide.
[0027] By iron oxide (Fe 2 o 3 ) by adding nickel oxide (Ni 2 o 3 ), zinc oxide (ZnO) and copper oxide (CuO) can be used to prepare NiCuZn soft magnetic ferrite, which has a high initial permeability and can be used for high-current inductors. Further add tricobalt tetroxide (Co 3 o 4 ), the resistance of the ferrite can be increased by cobalt tetroxide, thereby enhancing the ability of the ferrite to resist current impact.
[0028] Iron oxide, nickel oxide, zinc oxide, copper oxide and cobalt tetroxide are all commercially available. In this embod...
Embodiment 1
[0072] (1) Weigh the materials according to the following ratio (unit: g, tolerance: ±10%)
[0073] Material
Fe 2 o 3
Ni 2 o 3
ZnO
CuO
co 3 o 4
Deionized water
Zirconium ball
weight
62.77
8.44
19.67
9.02
0.10
100
400
[0074] The diameter of zirconium balls is 7mm, the mass ratio of pre-fired ingredients: balls: water is 1:4:1, the speed is 350 rpm, and ball milling is carried out for 4 hours. After discharging, drying, and passing through a 60-mesh sieve, put it in a mullite crucible, and prepare for pre-firing synthesis.
[0075] (2) Pre-fired synthesis
[0076] Pre-burning equipment: box furnace
[0077] Heating curve: starting from room temperature, the temperature is raised to 830°C at a rate of 2.5°C / min;
[0078] Heat preservation: keep heat at 830°C for 2.5 hours, close the box furnace, and cool the pre-fired powder to room temperature with the furnace.
[0079] (3) Weigh ...
Embodiment 2
[0090] (1) Weigh the materials according to the following ratio (unit: g, tolerance: ±10%)
[0091] Material
Fe 2 o 3
Ni 2 o 3
ZnO
CuO
co 3 o 4
Deionized water
Zirconium ball
weight
64.18
7.35
19.63
8.75
0.09
100
400
[0092] The diameter of zirconium balls is 7mm, the mass ratio of pre-fired ingredients: balls: water is 1:4:1, the speed is 350 rpm, and ball milling is carried out for 4 hours. After discharging, drying, and passing through a 60-mesh sieve, put it in a mullite crucible, and prepare for pre-firing synthesis.
[0093] (2) Pre-fired synthesis
[0094] Pre-burning equipment: box furnace
[0095] Heating curve: starting from room temperature, the temperature is raised to 855°C at a rate of 2.5°C / min;
[0096] Heat preservation: keep heat at 855°C for 2.5 hours, close the box furnace, and cool the pre-fired powder to room temperature with the furnace.
[0097] (3) Weigh ...
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