Carbon fiber composite material heating and curing process

A composite material and heat curing technology, which is applied in the field of carbon fiber composite material heat curing technology, can solve the problems of large residual stress of composite material components, component deformation, complex temperature field, etc., and achieve significant beneficial effects, high pass rate, and production cost control Effect

Inactive Publication Date: 2016-07-06
ANHUI JIALIQI AEROSPACE CARBON FIBER CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the other hand, the quality and production capacity of domestic carbon fiber are far from meeting the market demand, especially the high-quality carbon fiber composite materials in the civilian field, it is difficult to reach the world standard. Therefore, it is important to provide a stable carbon fiber production process. significance
[0004] In the production process of carbon fiber composite materials, due to the complex heat exchange and chemical reactions in the heating and curing process of composite materials, theoretically a temperature gradient will be generated inside the composite material, especially when the volume of the composite material is large, the difference in temperature gradient If it is too large, the internal residual stress of the composite material component will be too large, resulting in the deformation of the component
Usually, in the heating and curing process, it is necessary to cover the carbon fiber composite with auxiliary materials such as vacuum bags and air felts. These auxiliary materials play a role of heat insulation and have a complete temperature distribution on the surface near the mold and the surface near the vacuum bag. It is not the same, which also causes the temperature field in the hot pressing device to be more complicated, which also puts forward higher requirements for the all-round monitoring of the temperature in the hot pressing device during the heating and curing process

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Carry out the heating and curing process of carbon fiber composite materials according to the following steps:

[0023] Step 1, vacuumize, put the carbon fiber composite material into the curing device, vacuumize to less than -0.8bar, and maintain for 2min;

[0024] Step 2: pressurize and heat up, raise the ambient temperature in the curing device to 122°C, the temperature rise rate is 1.0°C / min, and pressurize to 1.2bar at the same time, when the temperature of the thermocouple on the composite material reaches 122°C, maintain the ambient temperature at all times 5°C higher than the temperature of the thermocouple;

[0025] Step 3, when the temperature of the thermocouple on the composite material in step 2 rises to 140°C, keep warm and pressurize, and under the pressure conditions of step 2, continue to pressurize to 3.5bar, and keep the constant pressure for 120min;

[0026] Step 4, lower the temperature and pressure, slowly lower the ambient temperature according t...

Embodiment 2

[0028] Carry out the heating and curing process of carbon fiber composite materials according to the following steps:

[0029] Step 1, vacuumize, put the carbon fiber composite material into the curing device, vacuumize to less than -0.8bar, and maintain for 5min;

[0030] Step 2: pressurize and heat up, raise the ambient temperature in the curing device to 125°C, the temperature rise rate is 2.0°C / min, and pressurize to 1.2bar at the same time, when the temperature of the thermocouple on the composite material reaches 122°C, maintain the ambient temperature at all times 4°C higher than the thermocouple temperature;

[0031] Step 3, when the temperature of the thermocouple on the composite material in step 2 rises to 140°C, keep warm and pressurize, and under the pressure conditions of step 2, continue to pressurize to 3.8bar, and keep the constant pressure for 100min;

[0032] Step 4, lower the temperature and pressure, slowly lower the ambient temperature according to the t...

Embodiment 3

[0034] Carry out the heating and curing process of carbon fiber composite materials according to the following steps:

[0035] Step 1, vacuumize, put the carbon fiber composite material into the curing device, vacuumize to less than -0.8bar, and maintain the time for 10min;

[0036] Step 2: pressurize and heat up, raise the ambient temperature in the curing device to 127°C, the temperature rise rate is 2.0°C / min, and pressurize to 2.0bar at the same time, when the temperature of the thermocouple on the composite material reaches 125°C, maintain the ambient temperature at all times 2°C higher than the thermocouple temperature;

[0037] Step 3, when the temperature of the thermocouple on the composite material in step 2 rises to 140°C, keep warm and pressurize, and under the pressure conditions of step 2, continue to pressurize to 4.0 bar and keep the pressure constant for 130 minutes;

[0038] Step 4, lower the temperature and pressure, slowly lower the ambient temperature acc...

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PUM

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Abstract

The invention relates to a carbon fiber composite material heating and curing process, and belongs to the technical field of carbon fiber composite material forming processes. The carbon fiber composite material heating and curing process comprises the following steps: (1) vacuumizing: a carbon fiber composite material is put in a curing device for vacuumizing to reach a vacuum degree of below -0.8 bar and keeping by 2-10 min; (2) pressurization and heating: the environmental temperature in the curing device rises to 120-170 DEG C at a speed of 1.0-2.0 DEGC / min; and meanwhile, the pressure rises to 1.0-2.0 bar; (3) insulation and pressurization: under the pressure condition in the step (2), the pressure continuously rises to 3.0-4.0 bar, and is kept by 100-150 min; and (4) cooling and pressure reduction: the environmental temperature is slowly reduced according to the temperature gradient of 8-12 DEG C; each temperature gradient is kept by 5-15 min; and when the environmental temperature is lower than 80 DEG C, the pressure is slowly reduced. The carbon fiber composite material, obtained by the technical scheme, is higher in product pass percent compared with a traditional process; the production cost is effectively controlled; and the beneficial effects are prominent.

Description

technical field [0001] The invention relates to a carbon fiber composite material heating and curing process, which belongs to the technical field of carbon fiber composite material forming technology. Background technique [0002] As an advanced composite material, carbon fiber composite material has a series of advantages such as light weight, high modulus, high specific strength, low thermal expansion coefficient, high temperature resistance, thermal shock resistance, corrosion resistance, and good vibration absorption. , strategic weapons (missiles, etc.) and other fields have been widely used. For example, if it is used in aerospace structures, it can reduce the weight by 20% to 30% compared with conventional metal structures, and can significantly improve its aeroelastic properties. It can effectively improve flight performance when used in the aerospace field, which is impossible or difficult to achieve with other materials. In the civilian field, the weight of carbo...

Claims

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Application Information

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IPC IPC(8): B29C70/44B29C70/54
CPCB29C70/44B29C70/54
Inventor 梁禹鑫路强
Owner ANHUI JIALIQI AEROSPACE CARBON FIBER CO LTD
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