Method for enhancing laser-induced breakdown spectroscopy intensity

A laser-induced breakdown and spectral intensity technology, applied in the field of femtosecond laser applications, can solve the problems of low analysis accuracy, complex experimental equipment, poor repeatability, etc., and achieve the effect of simple process and simple experimental optical path

Active Publication Date: 2016-06-22
BEIJING INSTITUTE OF TECHNOLOGYGY
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Problems solved by technology

However, compared with other analytical techniques, common LIBS technology has two major disadvantages: low analytical precision and poor repeatability
[0003] The above methods have their own disadvantages, such as the complex experimental optical path of the double-pulse method, and the need for additional equipment for EDM assistance, etc.
Patent CN105067572A discloses a method and device for enhancing laser-induced breakdown spectrum, which uses microwaves generated by a microwave generator to heat plasma to achieve spectral signal enhancement, but the experimental equipment for this method is relatively complicated; patent CN105067571A discloses a A device for enhancing the laser-induced breakdown spectrum. This invention enhances the spectral signal by changing the background gas and converging the plasma radiation with other devices, but the method is also complicated.

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  • Method for enhancing laser-induced breakdown spectroscopy intensity
  • Method for enhancing laser-induced breakdown spectroscopy intensity
  • Method for enhancing laser-induced breakdown spectroscopy intensity

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Embodiment

[0026] A method for enhancing the intensity of the laser-induced breakdown spectrum, specifically a method for enhancing the plasma radiation spectrum of a heat-resistant dielectric material assisted by femtosecond laser pulses ablated by gold nanoparticles, the femtosecond laser-induced breakdown processing optical path and spectrum Collection equipment such as figure 1 As shown, it includes two parts, the processing optical path and the spectrum acquisition equipment, wherein the processing optical path is the traditional femtosecond laser single pulse generated by the femtosecond laser 2. After the first mechanical switch 3 is opened, the femtosecond laser passes through the half-wave plate 4 and The ultra-fast polarizer 5 can adjust the power of the pulsed laser by adjusting the half-wave plate 4. The laser is focused on the surface of the sample 11 to be processed through the objective lens 10 to achieve ablation processing, and the three-dimensional mobile platform 12 rea...

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Abstract

The invention provides a method for enhancing laser-induced breakdown spectroscopy intensity, particularly relates to a method for promoting the absorption of a thermoelectric-medium-resistant material on femtosecond laser by using gold nanoparticles and further improving the plasma radiation spectroscopy intensity, and belongs to the technical field of femtosecond laser application. A layer of gold nanoparticle covers the surface of the thermoelectric-medium-resistant material by a hot dehumidifying method; in a region of focusing the femtosecond laser onto the surface of the material through a planoconvex lens, the material local electromagnetic field intensity is obviously enhanced due to the effect of plasma elements, so that the absorption mechanism of the thermoelectric-medium-resistant material on the femtosecond laser is changed; the volume of the plasma and the radiation spectroscopy intensity are finally improved. Under the condition of the same laser flux, the intensity of spectral lines is several times higher than that of the conventional femtosecond laser.

Description

technical field [0001] The invention relates to a method for enhancing the intensity of laser-induced breakdown spectrum, in particular to a method for using gold nanoparticles to promote the absorption of femtosecond laser by heat-resistant dielectric materials, thereby increasing the intensity of plasma radiation spectrum, which belongs to the application of femtosecond laser technology field. Background technique [0002] Laser-induced breakdown spectroscopy (LIBS for short) is an elemental analysis technique that uses a focusing lens to focus a pulsed laser, then excites a small amount of sample to generate plasma, and finally uses a spectrometer to analyze the resulting plasma. The spectral signals of different elements can be analyzed according to the characteristic spectrum. Because LIBS technology can basically analyze any element in any state, and can realize non-destructive testing and other advantages, LIBS technology has been widely used in fields such as minera...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/71
CPCG01N21/71
Inventor 姜澜杨帆王素梅曹志涛王猛猛
Owner BEIJING INSTITUTE OF TECHNOLOGYGY
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