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Integration equipment and detection method for evaluating coating bonding strength based on interface fracture toughness

A technology that combines strength and fracture toughness. It is applied in the directions of strength characteristics, testing material strength by applying stable tension/pressure, measuring devices, etc., to achieve the effects of simple preparation, clear equipment and detection principles, and beneficial modular design.

Active Publication Date: 2016-06-01
DALIAN UNIV OF TECH
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  • Application Information

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Problems solved by technology

[0004] In order to solve the engineering problem of quantitative detection of coating bonding strength, the present invention provides an integrated device and detection method for evaluating coating bonding strength based on interface fracture toughness. The ultrasonic non-destructive quantitative measurement of the amount is combined with the continuous indentation test of the coating-substrate interface. A single water immersion focused ultrasonic probe is used to simultaneously measure the shear wave and longitudinal wave sound velocities of the coating, and then obtain the Poisson's ratio of the coating to realize the elastic modulus of the coating. At the same time, the continuous loading process of the coating-substrate interface indentation test is controlled by the closed-loop acoustic emission signal. When the crack is formed, the loading is stopped according to the preset delay time, which simplifies the indentation test process and realizes the indentation test. Automatic identification of indentation tip cracks in equipment

Method used

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  • Integration equipment and detection method for evaluating coating bonding strength based on interface fracture toughness
  • Integration equipment and detection method for evaluating coating bonding strength based on interface fracture toughness
  • Integration equipment and detection method for evaluating coating bonding strength based on interface fracture toughness

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Embodiment 1

[0032] On the 316L stainless steel sample, HVOF high-speed flame thermal spraying WC-10Ni coating, after stress relief annealing heat treatment, measure the bonding strength. The detection method adopts the following steps:

[0033] 1) Preparation of coating sample and substrate sample: process the coating sample and substrate sample with the same shape and size as a cuboid, the thickness of the sample is 6mm, the length is 30mm, and the width is 15mm. The same long sample is cut off on the line, the thickness of the coating is 350 μm, the upper and lower surfaces of the sample are parallel and mechanically polished, the surface roughness is Ra=0.05 μm; the longitudinal cross-section of the coated sample is polished to a mirror surface for Metallographic measurement of coating thickness, porosity, microhardness measurement of coating and substrate, and indentation test of coating-substrate interface;

[0034] 2) Ultrasonic non-destructive measurement of the elastic modulus of ...

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Abstract

The invention discloses integration equipment and a detection method for evaluating coating bonding strength based on interface fracture toughness, belonging to the technical field of material surface engineering. With the equipment, a computer is used for controlling operation of four functional modules, including an ultrasonic detection module, a hardness testing module, a continuous press-in testing module and an interface crack detecting module; a man-machine interactive software system is used for processing acquisition and transmission of data of the functional modules and analysis operation and data display and output of an interface press-in mechanical model in an integrated manner; and through ultrasonic nondestructive measurement on elasticity modulus of a coating and a matrix and continuous press-in testing on a coating-matrix interface, quantitative detection on all parameters of an interface fracture toughness formula is completed in one equipment, and the critical load PC of coating-matrix interface fracture and the corresponding interface fracture toughness Kca are obtained. The equipment and the detection principle are clear, the modular design is beneficial to updating and expanding of a mechanical model library, and a detection sample is simple and convenient to prepare.

Description

technical field [0001] The invention relates to an integrated device and detection method for evaluating coating bonding strength based on interface fracture toughness, which is used for quantitative detection and evaluation of bonding strength of coatings of metals, alloys, ceramics and composite materials with a thickness of more than 100 μm, and belongs to material surface engineering technology field. technical background [0002] In recent years, surface coating technology has continued to develop and has gradually become a key means of manufacturing high-performance parts of major engineering equipment. Anti-fatigue and anti-oxidation protective coatings, as well as functional coatings such as electrical conductivity, magnetic conductivity, thermal conductivity, and electromagnetic shielding. The high reliability and long service life of these parts requires high bonding strength at the coating-substrate interface. At the same time, the thickness of the coating genera...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N19/04G01N3/06G01N3/42G01N3/08G01N29/07
CPCG01N3/068G01N3/08G01N3/42G01N19/04G01N29/07
Inventor 雷明凯朱小鹏林莉李昱鹏朱宝
Owner DALIAN UNIV OF TECH
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