Preparation method of novel oxycellulose hemostatic product
A technology for oxidizing cellulose and cellulose, applied in the fields of pharmaceutical formulation, application, medical science, etc., can solve problems such as harm to the human body and the environment, and achieve the effects of strong liquid absorption, soft texture, and increased specific surface area.
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Embodiment 1
[0038] Wood fiber is used as raw material, and the fiber fineness is 0.5 denier.
[0039] 1. The cellulose fibers are pretreated with a 1% sodium hydroxide solution, and after removing possible impurities, the surface of the fibers is further activated with an alkali solution.
[0040] 2. After pretreatment and activation, wash with deionized water until neutral, and air-dry the obtained cellulose product to obtain raw materials.
[0041] 3. Use 5% sodium hydroxide solution as a solvent, the dosage of cellulose product is 3% (in sodium hydroxide solution), then add 2% urea (in sodium hydroxide solution) and 2% ZnO ( (calculated as sodium hydroxide solution), fully dissolved at -15°C, and the system becomes viscose.
[0042] 4. After the fiber is completely dissolved in the solution and becomes viscose, slowly add the pore-forming agent sodium sulfate, and continue to stir for 20 minutes to make it a mixture of cellulose.
[0043] 5. Pour the cellulose mixture into the mold f...
Embodiment 2
[0055] Viscose fiber is used as raw material, and the fiber fineness is 1.0 denier.
[0056] 1. Pretreat the cellulose fibers with a 3% sodium hydroxide solution to remove impurities on the surface of the fibers, and then activate the surface of the fibers with an alkali solution.
[0057] 2. After pretreatment and activation, wash with deionized water until neutral, and air-dry the obtained cellulose product to obtain raw materials.
[0058] 3. Use 10% sodium hydroxide solution as a solvent, and the dosage of cellulose product is 5% (in sodium hydroxide solution), then add 2% urea (in sodium hydroxide solution) and 2% ZnO ( Calculated as sodium hydroxide solution), fully dissolved at -5°C, the system becomes viscose.
[0059] 4. After the fiber is completely dissolved in the solution and becomes viscose, slowly add the pore-forming agent sodium sulfate, and continue to stir for 20 minutes to make it a mixture of cellulose.
[0060] 5. Pour the cellulose mixture into the mol...
Embodiment 3
[0072] Cotton fiber is used as raw material, and the fiber fineness is 3.0 denier.
[0073] 1. Pretreat the cellulose fibers with a 5% sodium hydroxide solution, remove impurities on the surface of the fibers, and then activate the surface of the fibers with an alkali solution.
[0074] 2. After pretreatment and activation, wash with deionized water until neutral, and air-dry the obtained cellulose product to obtain raw materials.
[0075] 3. Use 20% sodium hydroxide solution as a solvent, the amount of cellulose product is 10% (in sodium hydroxide solution), then add 2% urea (in sodium hydroxide solution) and 2% ZnO ( (calculated as sodium hydroxide solution), fully dissolved at 5°C, and the system becomes viscose.
[0076] 4. After the fiber is completely dissolved in the solution and becomes viscose, slowly add the pore-forming agent sodium sulfate, and continue to stir for 20 minutes to make it a mixture of cellulose.
[0077] 5. Pour the cellulose mixture into the mold ...
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