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Quality control method of traditional Chinese medicine composition for treating chronic renal failure

A quality control method and technology of renal function, which can be used in measuring devices, instruments, scientific instruments, etc., to solve the problems of weak activity and single curative effect, and achieve the effects of good peak shape, improved analysis efficiency and good resolution.

Active Publication Date: 2016-05-04
SHENZHEN TRADITIONAL CHINESE MEDICINE HOSPITAL
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Problems solved by technology

But above-mentioned compound Chinese medicine curative effect is single, and activity is weak
[0004] Traditional Chinese medicine and its preparations are multi-component complex systems, so the evaluation of their quality should adopt appropriate quality control methods that can provide rich identification information, but the current methods of microscopic identification, physical and chemical identification and content determination are not enough to solve this problem

Method used

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  • Quality control method of traditional Chinese medicine composition for treating chronic renal failure
  • Quality control method of traditional Chinese medicine composition for treating chronic renal failure
  • Quality control method of traditional Chinese medicine composition for treating chronic renal failure

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preparation example Construction

[0024] The preparation method of the above-mentioned traditional Chinese medicine composition for treating chronic renal failure comprises the steps of: pulverizing Atractylodes macrocephala, Chinese yam and cardamom in the raw materials into fine powder for later use; , roasted licorice, add water to decoct twice, add 10 times the weight of water for the first time, add 8 times the weight of water for the second time, decoct for 1 hour each time, filter the decoction, combine the filtrates, and concentrate until the relative density is The thick ointment of 1.20, let cool, mix with described fine powder, pelletize after the mixing, dry, coat, dry, pack, obtain the pill of the Chinese medicine composition for the treatment of chronic renal failure.

[0025] The above-mentioned prescription of the present invention is based on clinically proven prescriptions, and on the basis of the original decoction, it is researched into a pill with simple process and definite curative effect...

Embodiment 1

[0033] The quality control method of the above-mentioned Chinese medicine composition for the treatment of chronic renal failure

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Abstract

The invention relates to the technical field of a traditional Chinese medicine preparation, and particularly relates to a quality control method of a traditional Chinese medicine composition for treating chronic renal failure. The quality control method comprises the following steps: establishing a fingerprint spectrum of the traditional Chinese medicine composition by adopting a high performance liquid chromatography with the chromatographic condition of taking octadecyl silane as a filling agent, taking a 0.2% phosphoric acid solution as a mobile phase A and taking acetonitrile as a mobile phase B; preparing a test solution, namely, putting 0.1-1g of the traditional Chinese medicine composition for treating chronic renal failure into a 50ml of a centrifugal pipe, adding 5-20ml of ultrapure water, carrying out ultrasound treatment for 10-30 minutes, cooling, mixing evenly, then centrifuging, taking liquid supernatant, filtering by a 0.45micron of microporous filtering membrane, and taking subsequent filtrate to obtain a test solution; and determining, namely, sucking the test solution precisely, pouring into a liquid chromatograph, and recording a chromatogram. The quality control method is rapid, simple, and convenient; by adopting once extraction and simultaneous determining, the operation steps are reduced, the time and cost are saved, and thus the analysis efficiency is improved.

Description

technical field [0001] The invention relates to the technical field of traditional Chinese medicine preparations, in particular to a quality control method of a traditional Chinese medicine composition for treating chronic renal failure. Background technique [0002] At present, traditional Chinese medicine has unique features in disease prevention and treatment. Chronic renal failure belongs to the categories of edema, dysentery, and off-grade in Chinese medicine. The pathogenesis is based on deficiency in origin and excess in superficiality. Although dialysis or kidney transplantation is the treatment for the end-stage survival of patients with chronic renal failure, in the early and middle stages of chronic renal failure, on the basis of treating the primary disease, effective drug treatment measures can be used to effectively prevent or delay the disease. Progression of chronic renal failure is an ideal method. [0003] Studies have shown that traditional Chinese medic...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/86G01N30/74G01N30/06
CPCG01N30/06G01N30/74G01N30/8686
Inventor 陈剑平李顺民张尚斌郑平何泰东余晓丹
Owner SHENZHEN TRADITIONAL CHINESE MEDICINE HOSPITAL
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