Making method of graphene oxide-containing antibiosis and mildew prevention wallpaper
A technology of antibacterial and antifungal, antibacterial and antifungal agent, applied in the fields of botanical equipment and methods, preparation of ether, special paper, etc., to achieve excellent bactericidal performance, improvement of home environment, and low cost
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Embodiment 1
[0020] Isolation, preparation and structure confirmation of wild lily extract compounds:
[0021] Preparation method: (a) The dried whole herb of Wild Lily (10kg) is pulverized, extracted with 80% ethanol under heat reflux (25L×3 times), the extracts are combined, concentrated to no alcohol smell (3L), and successively washed with petroleum ether (3L ×3 times), ethyl acetate (3L×3 times) and water-saturated n-butanol (3L×3 times) were extracted to obtain petroleum ether extract, ethyl acetate extract (398g) and n-butanol extract respectively; (b) In the step (a), the ethyl acetate extract is removed with AB-8 type macroporous resin, first eluted with 10% ethanol for 8 column volumes, then with 75% ethanol for 10 column volumes, and collected 75 % ethanol eluate, concentrated under reduced pressure to obtain 75% ethanol eluate extract (163g); (c) 75% ethanol eluate extract in step (b) is separated with 200-300 mesh normal phase silica gel, and the volume The ratios are 85:1 (8...
Embodiment 2
[0024] A method for preparing graphene oxide-containing antibacterial and mildew-resistant wallpaper, the method comprising: uniformly distributing the prepared antibacterial and anti-mildew agent on the base paper through a spraying process to obtain the anti-bacterial and anti-mildew enzyme wallpaper.
[0025] The antibacterial and antifungal agent includes, in parts by weight: 0.5 parts of nano-graphene oxide, 2.3 parts of nano-cerium oxide, 0.01 part of wild lily extract compound, 1.0 part of polyethylene glycol, 0.2 part of polyvinylpyrrolidone, and 20 parts of water.
[0026] The nano-graphene oxide has a purity of ≥95%, a sheet thickness of 0.5nm, and a sheet length of 100nm.
[0027] The structural formula of the wild lily extract compound is and the preparation method is the same as in Example 1.
[0028] The preparation method of the antibacterial and antifungal agent specifically includes the following steps: (a) under the action of ultrasonic waves, successively ad...
Embodiment 3
[0032] A method for preparing graphene oxide-containing antibacterial and antibacterial wallpaper, the method comprising: uniformly distributing the prepared antibacterial and antifungal agent on the base paper through a spraying process to obtain the antibacterial and antifungal wallpaper.
[0033] The antibacterial and antifungal agent includes, in parts by weight: 4.35 parts of nano-graphene oxide, 5.5 parts of nano-cerium oxide, 1.65 parts of wild lily extract compound, 5.5 parts of polyethylene glycol, 1.8 parts of polyvinylpyrrolidone, and 80 parts of water.
[0034] The nano-graphene oxide has a purity of ≥95%, a sheet thickness of 2nm, and a sheet length of 800nm.
[0035] The structural formula of the wild lily extract compound is and the preparation method is the same as in Example 1.
[0036] The preparation method of the antibacterial and antifungal agent specifically includes the following steps: (a) under the action of ultrasonic waves, successively add polyethyl...
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