Technology for preparation of low-magnesium phosphate concentrate and byproducts calcium carbonate and magnesium oxide from medium and low grade phosphate rock
A low-magnesium phosphorus concentrate, low-grade technology, applied in the direction of magnesium oxide, calcium carbonate/strontium/barium, phosphate material treatment, etc., can solve the problems of land occupation and processing difficulties, to solve the problem of land occupation and environmental protection Pollution, effect of reducing magnesium content
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Embodiment 1
[0041] A process for producing low-magnesium phosphorus concentrate by-product calcium carbonate and magnesium oxide from medium and low-grade phosphate rock, the process flow chart is as follows figure 1 shown, including the following steps:
[0042] (1) Calcining 100g of low- and medium-grade phosphate rock at 900-1100°C for 1 hour (the factory calcination process is to mix low- and medium-grade phosphate rock with anthracite for calcination) to obtain calcined slag and carbon dioxide; Dolomite (CaCO 3 · MgCO 3 ), calcite (CaCO 3 ) and fluorapatite (Ca 5 F(PO 4 ) 3 ), where dolomite and calcite begin to decompose at high temperatures above 750°C, as follows:
[0043] CaCO 3 · MgCO 3 =CaO+MgO+2CO 2
[0044] CaCO 3 =CaO+CO 2
[0045] At the same time, fluoroapatite (Ca 5 F(PO 4 ) 3 ) has a decomposition temperature of 1650°C and will not decompose in the range of 900-1100°C;
[0046] (2) Digest the calcined slag with water at 60°C; using higher temperature water...
Embodiment 2
[0068] A process for producing low-magnesium phosphorus concentrate by-product calcium carbonate and magnesium oxide from medium and low-grade phosphate rock, the process flow chart is as follows figure 1 shown, including the following steps:
[0069] (1) Calcining 100g of low- and medium-grade phosphate rock at 900-1100°C for 2 hours to obtain calcined slag and carbon dioxide; studies have shown that dolomite (CaCO 3 · MgCO 3 ), calcite (CaCO 3 ) and fluorapatite (Ca 5 F(PO 4 ) 3 ), where dolomite and calcite begin to decompose at high temperatures above 750°C, as follows:
[0070] CaCO 3 · MgCO 3 =CaO+MgO+2CO 2
[0071] CaCO 3 =CaO+CO 2
[0072] At the same time, fluoroapatite (Ca 5 F(PO 4 ) 3 ) has a decomposition temperature of 1650°C and will not decompose in the range of 900-1100°C;
[0073] (2) Digest the calcined slag with water at 100°C; using higher temperature water can accelerate the reaction of CaO and MgO with water to form calcium hydroxide and m...
Embodiment 3
[0085]A process for producing low-magnesium phosphorus concentrate by-product calcium carbonate and magnesium oxide from medium and low-grade phosphate rock, the process flow chart is as follows figure 1 shown, including the following steps:
[0086] (1) Calcining 100g of low- and medium-grade phosphate rock at 900-1100°C for 1.5 hours to obtain calcined slag and carbon dioxide; studies have shown that dolomite (CaCO 3 · MgCO 3 ), calcite (CaCO 3 ) and fluorapatite (Ca 5 F(PO 4 ) 3 ), where dolomite and calcite begin to decompose at high temperatures above 750°C, as follows:
[0087] CaCO 3 · MgCO 3 =CaO+MgO+2CO 2
[0088] CaCO 3 =CaO+CO 2
[0089] At the same time, fluoroapatite (Ca 5 F(PO 4 ) 3 ) has a decomposition temperature of 1650°C and will not decompose in the range of 900-1100°C;
[0090] (2) Digest the calcined slag with water at 80°C; using higher temperature water can accelerate the reaction of CaO and MgO with water to form calcium hydroxide and m...
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