A composite material for toughening concrete
A composite material and concrete technology, applied in the field of toughened composite material preparation, can solve the problems of affecting the service life and safety of buildings, prone to cracks, low flexural strength, etc. processing effect
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Embodiment 1
[0034]First prepare modified silica nanotubes:
[0035] (1) Put 30 stainless steel balls with a diameter of 10 mm and 45 stainless steel balls with a diameter of 5 mm in two identical 5 L nylon tanks, then add 0.9 kg of silica nanotubes respectively, and then drop Add 90 ml absolute ethanol and seal with a nylon cap. Put two ball mill jars symmetrically into the ball mill, and ball mill them for 48 h under the condition that the rotation speed is 400 rpm and the rotation direction is automatically switched every 30 minutes;
[0036] (2) Add the silica nanotubes treated in step (1) into an aqueous solution of Tween 20 with a pH of 8 and a concentration of 20 wt%, sonicate for 18 h, filter, wash with water, and vacuum at 55°C Dry for 15 hours;
[0037] (3) Take the silica nanotubes treated in step (3) and stir in 40 L of 35wt% sodium hydroxide aqueous solution for 48 hours, filter, wash the powder with pure water, and vacuum at 60°C Dry for 18 hours;
[0038] (4) Take the si...
Embodiment 2
[0048] First prepare modified silica nanotubes:
[0049] (1) Put 30 stainless steel balls with a diameter of 10 mm and 45 stainless steel balls with a diameter of 5 mm in two identical 5 L nylon tanks, then add 0.9 kg of silica nanotubes respectively, and then drop Add 90 ml of absolute ethanol and seal it with a nylon cover; put two ball mill jars into the ball mill symmetrically, and ball mill for 48 h under the condition that the rotation speed is 400 rpm and the rotation direction is automatically changed every 30 minutes;
[0050] (2) Add the silica nanotubes treated in step (1) into an aqueous solution of Tween 20 with a pH of 8 and a concentration of 20 wt%, sonicate for 18 h, filter, wash with water, and vacuum at 57°C Dry for 15 hours;
[0051] (3) Take the silica nanotubes treated in step (2) and stir in 40 L of 35wt% sodium hydroxide aqueous solution for 48 hours, filter, wash the powder with pure water, and vacuum at 59°C Dry for 18 hours;
[0052] (4) Take the ...
Embodiment 3
[0062] First prepare modified silica nanotubes:
[0063] (1) Put 30 stainless steel balls with a diameter of 10 mm and 45 stainless steel balls with a diameter of 5 mm in two identical 5 L nylon tanks, then add 0.9 kg of silica nanotubes respectively, and then drop Add 90 ml of absolute ethanol and seal it with a nylon cover; put two ball mill jars into the ball mill symmetrically, and ball mill for 48 h under the condition that the rotation speed is 400 rpm and the rotation direction is automatically changed every 30 minutes;
[0064] (2) Add the silica nanotubes treated in step (1) into an aqueous solution of Tween 20 with a pH of 8 and a concentration of 20 wt%, sonicate for 18 h, filter, wash with water, and vacuum at 56°C Dry for 15 hours;
[0065] (3) Take the silica nanotubes treated in step (2) and stir in 40 L of 35 wt% sodium hydroxide aqueous solution for 48 hours, filter, wash the powder with pure water, and vacuum at 60°C Dry for 18 hours;
[0066] (4) Take the...
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