A kind of special latex for non-sticking lid of yogurt and its preparation method and application
A seed latex and latex technology, which is applied in the field of polymer materials, can solve the problem of yogurt being easily adhered to the yogurt cover, and achieve the effects of reducing the residual amount of monomers, improving the vacuum desorption effect and uniform particle size distribution.
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Embodiment 1
[0021] (1) Mixed monomer preparation: mix 80kg of vinylidene chloride, 12kg of methyl methacrylate, 7kg of methyl chlorosilane, 0.3kg of beeswax and 0.7kg of methacrylic acid, stir at high speed for 2 hours, and set aside;
[0022] (2) Emulsifier preparation: dilute 2 kg of sodium paraffin sulfonate with deionized water to 20 kg, stir and mix at high speed, and set aside;
[0023] (3) Initiator preparation: the sodium persulfate 160g is added in deionized water 8kg and stirred and mixed to make an initiator solution, for subsequent use;
[0024] (4) Seed polymerization reaction: Add 64kg of deionized water or soft water, 24g of auxiliary ammonium acetate, 1g of ferrous chloride, and 120g of seed polymerization emulsifier sodium dodecylbenzenesulfonate into a 200L reaction kettle, seal the kettle, and use Nitrogen replacement 5 times, vacuuming, inhalation of 5% (weight) of the mixed monomer prepared in step 1, cold dispersion for 1h, heating up to 45°C, and continuously pumpin...
Embodiment 2
[0028] (1) Mixed monomer preparation: mix 82 kg of vinylidene chloride, 8 kg of methyl methacrylate, 9 kg of phenylchlorosilane, 0.4 kg of beeswax and 0.6 kg of methacrylic acid, stir at high speed for 2 hours, and set aside;
[0029] (2) Emulsifier preparation: dilute 3 kg of sodium paraffin sulfonate with deionized water to 20 kg, stir and mix at high speed, and set aside;
[0030] (3) Initiator preparation: the sodium persulfate 180g is added in deionized water 8kg and stirred and mixed to make an initiator solution, for subsequent use;
[0031] (4) Seed polymerization reaction: Add 64kg of deionized water or soft water, 24g of auxiliary ammonium acetate, 1g of ferrous chloride, and 140g of seed polymerization emulsifier sodium dodecylbenzenesulfonate into a 200L reaction kettle, seal the kettle, and use Nitrogen replacement 5 times, vacuuming, inhalation of 5% (weight) of the mixed monomer prepared in step 1, cold dispersion for 1h, heating up to 45°C, and continuously pum...
Embodiment 3
[0035] (1) Mixed monomer preparation: mix 83kg of vinylidene chloride, 10kg of methyl methacrylate, 6kg of methyl vinyl chlorosilane, 0.4kg of beeswax and 0.6kg of methacrylic acid, stir at high speed for 2 hours, and set aside;
[0036] (2) Emulsifier preparation: dilute 4 kg of sodium paraffin sulfonate with deionized water to 20 kg, stir and mix at high speed, and set aside;
[0037] (3) Initiator preparation: the sodium persulfate 200g is added in deionized water 8kg and stirred and mixed to make an initiator solution, for subsequent use;
[0038] (4) Seed polymerization reaction: Add 64kg of deionized water or soft water, 24g of auxiliary ammonium acetate, 1g of ferrous chloride, and 160g of seed polymerization emulsifier sodium dodecylbenzenesulfonate into a 200L reaction kettle, seal the kettle, and use Nitrogen replacement 5 times, vacuuming, inhalation of 5% (weight) of the mixed monomer prepared in step 1, cold dispersion for 1h, heating up to 45°C, and continuously ...
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