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Compound functional black coloring agent and preparation method thereof

A technology of compound function and dyeing agent, applied in the direction of dyeing physical treatment, chemical instruments and methods, dyeing organic silicon compound treatment, etc. , The effect of simple operation process and low production cost

Active Publication Date: 2016-01-20
延安金瓯科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This traditional process has a certain effect on reducing the dyeing cost of phenolic molding compounds; but it has certain limitations on the dispersion and utilization of carbon black
The main disadvantages are as follows: (1) The dosage is relatively large; (2) The dispersion is uneven; (3) The appearance of the product is not beautiful; (4) The product is brittle; (5) It affects the curing speed of phenolic resin; (6) It is easy to pollute the production process

Method used

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  • Compound functional black coloring agent and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A composite functional black dyeing agent of model F081-A was prepared. It is prepared from the following raw materials in parts by weight: 0.1 part of nano-calcium carbonate, 0.3 part of nano-montmorillonite, 6 parts of pigment carbon black, 0.1 part of dispersant, 0.1 part of lubricant, 0.01 part of defoamer, and 0.2 part of emulsifier part, 0.2 part of coupling agent.

[0023] The preparation method of the composite function black dyeing agent of model F081-A, carry out as follows:

[0024] Step 1: Pre-dispersion

[0025] Put nano-calcium carbonate and nano-montmorillonite in a high-speed mixer; add dispersant, lubricant, and stir at high speed for 1-3 minutes; then add coupling agent and continue stirring for 1-2 minutes; then add pigment carbon black , and continue stirring for 5-8 minutes, keeping the temperature at 25°C~45°C.

[0026] Step 2: Ball Mill Dispersion or Ultrasonic Dispersion

[0027] Put the material obtained in step 1 into a ball mill or ultraso...

Embodiment 2

[0031] A composite functional black dyeing agent of model F082-A was prepared. It is prepared from the following raw materials in parts by weight: 0.1 part of nano-montmorillonite, 0.4 part of nano-silica, 8 parts of pigment carbon black, 0.1 part of dispersant, 0.15 part of lubricant, 0.01 part of defoamer, emulsifier 0.1 part, 0.2 part of coupling agent.

[0032] The preparation method of the composite function black dyeing agent of model F082-A, carry out as follows:

[0033] Step 1: Pre-dispersion

[0034] Put nano-montmorillonite and nano-silica in a high-speed mixer; add dispersant, lubricant, and stir at high speed for 1-3 minutes; then add coupling agent and continue stirring for 1-2 minutes; then add pigment carbon black, continue to stir for 5-8 minutes, and keep the temperature at 25°C~45°C.

[0035] Step 2: Ball Mill Dispersion or Ultrasonic Dispersion

[0036] Put the material obtained in step 1 into a ball mill or ultrasonic dispersion equipment for further d...

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Abstract

Provided are a compound functional black coloring agent and a preparation method thereof. The compound functional black coloring agent is prepared from, by weight, 0.1-0.7 part of inorganic nano-materials, 6-8 parts of color black, 0.1 part of dispersing agent, 0.1-0.15 part of lubricating agent, 0.01 part of antifoaming agent, 0.1-0.2 part of emulgator and 0.2 part of coupling reagent. The preparation method comprises the following steps of 1, pre-dispersion, wherein nano particles, the dispersing agent and the lubricating agent are stirred at high speed for 1-3 minutes, the coupling reagent is added to be stirred for 1-2 minutes, and then the color black is added to be stirred for 5-8 minutes; 2, ball-milling dispersion or ultrasonic dispersion; 3, emulsification treatment, wherein the emulgator, the antifoaming agent and a proper amount of process water are added for low-speed stirring. According to the compound functional black coloring agent, the nano-material, namely, the modified color black is adopted, and the advantages of being good in dispersion performance, high in dyeing property, low in production cost, stable in property and the like are achieved. According to the preparation method, the operating process is easy and convenient.

Description

technical field [0001] The invention relates to a composite functional black dyeing agent and a preparation method thereof, in particular to a composite functional black dyeing agent modified with nanomaterials to pigment carbon black and a preparation method thereof. Background technique [0002] Phenolic resin is a polymer material that is polymerized with phenol and formaldehyde as raw materials under the condition of acidic catalyst (or basic catalyst). Its production process is stable and easy to operate, the price of raw materials is low, and it has many advantages such as good heat resistance, electrical insulation, corrosion resistance, low smoke generation, and product dimensional stability. Therefore, phenolic molding compound (commonly known as bakelite powder) with phenolic resin as the main raw material is widely used in many fields such as household appliances, household cooking utensils, aerospace, and automobile industry. Among the many phenolic molding prod...

Claims

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Application Information

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IPC IPC(8): C08L61/06C08K9/06C08K9/02C08K9/00C08K3/04C09C1/48C09C3/12C09C3/06C09C3/04C09C3/00
Inventor 范忠庆姚建明黄振贻
Owner 延安金瓯科技发展有限公司
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