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A kind of liquid barium/zinc thermal stabilizer, its preparation method and equipment for implementing the method

A thermal stabilizer and liquid technology, which is applied in the field of liquid barium/zinc thermal stabilizer, can solve the problems of great harm to operators, long production time period, cumbersome production steps, etc., achieve short production cycle, simplify production process, reduce unnecessary The effect of the safety factor

Active Publication Date: 2017-09-22
GUANGZHOU YINGSU NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Its disadvantages are: 1. The production steps are cumbersome and the process is complicated, including feeding, salt formation, dehydration, compounding, pressure filtration, and finished product packaging processes. Each process is completed in different equipment, and semi-finished products need to be manually transferred. It is very troublesome; 2. Production The time period is long and the energy consumption is high, especially the dehydration and the two production processes of the filter press consume a lot of energy; 3. A large amount of acid mist is formed during high-temperature production, and the production of the equipment is not closed, which is harmful to the operators; 4. The new formula is new In the process, there is no bisphenol A and nonylphenol prohibited by the European Union, and the thermal stability time and processing performance have been significantly improved compared with the previous process

Method used

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  • A kind of liquid barium/zinc thermal stabilizer, its preparation method and equipment for implementing the method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0054] A liquid barium / zinc heat stabilizer, comprising the following preparation raw materials in parts by weight: 28 parts of barium hydroxide monohydrate, 15 parts of zinc oxide, 33 parts of acid solution, 1 part of catalyst, 2 parts of water-carrying agent, saturated cycloalkane solvent 18 parts, 10 parts of heat-resistant additive;

[0055] Among them, the acid solution is a mixture of 5 parts of isooctanoic acid, 10 parts of octanoic acid, 5 parts of oleic acid, 10 parts of p-tert-butylbenzoic acid and 3 parts of benzoic acid, the catalyst is a mixture of 0.3 parts of acetic acid and 0.7 parts of formic acid, and the water carrier It is a mixture of 1 part of ethylene glycol and 1 part of methanol, the saturated naphthenic solvent is a mixture of 3 parts of glycerin, 2 parts of methyl ethyl ketone, 8 parts of odorless kerosene and 5 parts of albino oil, and the heat-resistant additive is 5 parts of soybean oil and a mixture of 5 parts phosphite.

[0056] A preparation m...

Embodiment 2

[0063] A liquid barium / zinc heat stabilizer, comprising the following preparation raw materials in parts by weight: 30 parts of barium hydroxide monohydrate, 17 parts of zinc oxide, 38 parts of acid solution, 1 part of catalyst, 1 part of water-carrying agent, saturated cycloalkane solvent 5 parts, 5 parts of heat-resistant additive;

[0064] Among them, the acid liquid is 38 parts of oleic acid, the catalyst is 1 part of propionic acid, the water-carrying agent is 1 part of ethylene glycol, the saturated naphthenic solvent is 5 parts of deodorized kerosene, and the heat-resistant additive is 2 parts of SBM and 3 parts of DBM. mixture.

[0065] A preparation method of liquid barium / zinc heat stabilizer, comprising the following steps:

[0066] 201. Pre-heat the oil bath temperature of the reactor to 140°C, add 38 parts of acid solution into the reactor, cover the lid of the reactor, start stirring and heat the temperature to 95°C, and the stirring frequency is 18Hz per minute...

Embodiment 3

[0072] A liquid barium / zinc heat stabilizer, comprising the following preparation raw materials in parts by weight: 30 parts of barium hydroxide monohydrate, 15 parts of zinc oxide, 40 parts of acid solution, 1 part of catalyst, 1 part of water-carrying agent, saturated cycloalkane solvent 8 parts, 5 parts heat-resistant additive;

[0073] Among them, the acid liquid is a mixture of 18 parts of isooctanoic acid and 22 parts of p-tert-butylbenzoic acid, the catalyst is a mixture of 0.5 parts of acetic acid, 0.2 parts of formic acid and 0.3 parts of propionic acid, and the water carrier is 1 part of methanol, saturated naphthenic solvent It is a mixture of 3 parts of triethylene glycol and 5 parts of cyclohexanone, and the heat-resistant additive is a mixture of 2 parts of soybean oil, 2 parts of phosphite ester and 1 part of antioxidant.

[0074] A preparation method of liquid barium / zinc heat stabilizer, comprising the following steps:

[0075] 301. Pre-heat the oil bath temp...

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Abstract

The invention discloses a liquid barium / zinc heat stabilizer. The liquid barium / zinc heat stabilizer comprises the following preparation raw materials in parts by weight: 20-30 parts of barium oxide and / or barium hydroxide, zinc oxide and / or Or 15-20 parts of zinc hydroxide, 30-40 parts of acid solution, 1-2 parts of water-carrying agent, 5-20 parts of saturated naphthenic solvent and 5-15 parts of heat-resistant additive, and the hydroxide of barium is anhydrous At least one of barium hydroxide, barium hydroxide monohydrate and barium hydroxide octahydrate. The invention also discloses a preparation method of the liquid barium / zinc heat stabilizer and equipment for implementing the method. The performance of the liquid barium / zinc heat stabilizer of the present invention is stable, the product has no pungent smell, and will not cause harm to the health of operators; the preparation method of the liquid barium / zinc heat stabilizer of the present invention adopts a one-step method, which simplifies production The technology reduces the unsafe factors in the production process and improves the production efficiency and output rate.

Description

technical field [0001] The invention belongs to the field of liquid stabilizers, and in particular relates to a liquid barium / zinc heat stabilizer, a preparation method thereof and equipment for implementing the method. Background technique [0002] With the rise of the PVC market, heat stabilizers as the main processing aids have undergone revolutionary changes. Since the industry was first developed, it was widely used in high-transparency liquid barium-cadmium-zinc and barium-cadmium paste heat stabilizers. With the rise of EU environmental protection requirements and Sony Electronics requirements, more and more countries have begun to use liquid barium-cadmium-zinc and barium Restricted use or prohibition of cadmium paste heat stabilizers. In this way, agricultural films, transparent shoe soles, car floor mats, and high-transparency toy materials that were widely used in the past are gradually replaced by liquid barium-zinc heat stabilizers. [0003] At present, the pr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L27/06C08L91/00C08K5/00C08K5/098C08K5/524B01J19/18
Inventor 李俭
Owner GUANGZHOU YINGSU NEW MATERIAL TECH CO LTD
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