Preparation method of medical pressure sensitive adhesive (PSA)
A pressure-sensitive adhesive and butyl rubber technology, applied in the direction of rosin adhesives, adhesive additives, non-polymer adhesive additives, etc., can solve the problems of incomplete peeling, poor stickiness, and large peeling force, and achieve Excellent adhesion and persistence, good integrity, and easy peeling effect
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Embodiment 1
[0017] A preparation method of medical pressure-sensitive adhesive, the steps are as follows:
[0018] Step 1: Add 2 parts by weight of butyl rubber, 7 parts of rosin glyceride, 6001 parts of polyethylene glycol, 1 part of calcium lignosulfonate, and 2 parts of sodium alginate into a mixer and stir and mix evenly, wherein The stirring speed of stirring and mixing is 100 rpm, the stirring time is 20 minutes, and the material 1 is obtained;
[0019] Step 2: Add 2 parts of diethyl phosphite and 3 parts of chlorinated paraffin into the material 1, mix evenly and then knead, the kneading temperature is 130°C, the kneading time is 30 minutes, and the kneaded product is obtained;
[0020] Step 3: Add 2 parts of maleamic acid and 3 parts of methacrylic acid to the kneading mixture, heat and stir for 30 minutes in the presence of nitrogen, and then knead again. The kneading temperature is 130°C and the kneading time is For 20 minutes, a medical pressure-sensitive adhesive is obtained....
Embodiment 2
[0022] A preparation method of medical pressure-sensitive adhesive, the steps are as follows:
[0023] Step 1, 3 parts by weight of butyl rubber, 8 parts of rosin glyceride, 8002 parts of polyethylene glycol, 2 parts of calcium lignosulfonate, and 3 parts of sodium alginate are added to the mixer and stirred and mixed evenly, wherein The stirring speed of stirring and mixing is 105 rpm, and the stirring time is 23 minutes, and the material 1 is obtained;
[0024] Step 2: Add 3 parts of diethyl phosphite and 5 parts of chlorinated paraffin into the material 1, mix evenly and then knead, the kneading temperature is 134°C, the kneading time is 38 minutes, and the kneaded product is obtained;
[0025] Step 3: Add 3 parts of maleamic acid and 4 parts of methacrylic acid to the mixture, heat and stir for 36 minutes in the presence of argon, and then carry out mixing. The mixing temperature is 133°C. The time is 25 minutes, and the medical pressure-sensitive adhesive is obtained.
Embodiment 3
[0027] A preparation method of medical pressure-sensitive adhesive, the steps are as follows:
[0028] Step 1, 5 parts by weight of butyl rubber, 8 parts of rosin glyceride, 8004 parts of polyethylene glycol, 2 parts of calcium lignosulfonate, and 3 parts of sodium alginate are added to the mixer and stirred evenly, wherein The stirring speed of stirring and mixing was 110 rpm, and the stirring time was 27 minutes to obtain material 1;
[0029] Step 2: Add 4 parts of diethyl phosphite and 6 parts of chlorinated paraffin into the material 1, mix evenly and then knead, the kneading temperature is 138°C, the kneading time is 42 minutes, and the kneaded product is obtained;
[0030] Step 3: Add 4 parts of maleamic acid and 5 parts of methacrylic acid to the mixture, heat and stir for 45 minutes in the presence of nitrogen, and then carry out mixing. The mixing temperature is 137°C and the mixing time is For 28 minutes, a medical pressure-sensitive adhesive was obtained.
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