Water decomposition photocatalyst, preparation method and applications thereof
A technology of catalysts and composite catalysts, applied in chemical instruments and methods, physical/chemical process catalysts, chemical/physical processes, etc., can solve problems such as poor stability and low quantum efficiency of photocatalysts, and achieve good stability.
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[0044] The method of the present invention will be described below through specific examples, but the present invention is not limited thereto. The experimental methods described in the following examples, unless otherwise specified, are conventional methods; the reagents and materials, unless otherwise specified, can be obtained from commercial sources.
[0045] The present invention is pyrolysis urea synthesis C3 N 4 method to prepare CDots-C by compounding carbon nanodots 3 N 4 Composite nano-catalysts realize visible light catalytic water splitting. In this specification, CDots all represent carbon quantum dots.
[0046] Prepare CDots;
[0047] CDots were synthesized by electrochemical etching. Two graphite rods were inserted into ultrapure water as anode and cathode, and a DC voltage of 30 V was applied between the two electrodes, and the reaction was continued for 120 h under constant stirring. After the reaction, the colorless ultrapure water turns dark yellow. ...
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