Thin polymer film preparation process
A technology of polymer film and preparation process, which is applied in the field of film manufacturing, and can solve problems such as alignment misalignment, difficulty, and device size deviation in the edge area
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Embodiment 1
[0029] combine figure 1 , describe in detail the preparation process of a polymer film of the present invention, including:
[0030] (1) Pre-coating, coating a polymer precursor solution on a carrier substrate to form a primary film. The polymer precursor solution in the step (1) of the present invention is a high-viscosity solution, and the viscosity range of the solution is 800cp-20000cp. For the viscosity range of the solution is 3000cp~5000cp, the technological effect of the present invention is better.
[0031] Specifically, the polymer precursor solution can be coated by blade coating, slit coating, spray coating or screen printing, and the thickness of the primary film is preferably 1 um to 1000 um.
[0032] After the pre-coating is completed, proceed to step (2).
[0033] (2) Centrifugal thick side adjustment, the carrier substrate in step (1) is transferred to the spin coating device together with the primary film coated thereon, and the spin coating device makes t...
Embodiment 2
[0044] In order to verify the effect of the present invention, two samples were prepared by the process of the present invention for performance research.
[0045] The specific preparation process of sample 1 is as follows:
[0046] (1) Select clean white glass as the carrier substrate, and use conventional cleaning process for cleaning.
[0047] (2) Scrape polyamic acid solution on white glass at a speed of 30mm / s to form a primary film. The viscosity of the polyamic acid solution is 3000cP, and the thickness of the primary film is about 0.5mm.
[0048] (3) Use a spin coating device to rotate at a speed of 500r / min for 12s, and then rotate at a speed of 1000r / min for 30s to adjust the centrifugal thickness.
[0049] (4) Send the primary film and the carrier substrate after the centrifugal thickening adjustment into the N 2 The polyamic acid primary film is cured and formed into a film in an oven in an atmosphere. The temperature control process of the oven is as follows: hea...
Embodiment 3
[0067] Adopt technology of the present invention to prepare sample 3, the concrete preparation process of sample 3 is as follows:
[0068] (1) Select clean white glass as the carrier substrate, and use conventional cleaning process for cleaning.
[0069] (2) Spray the polyamic acid solution on the white glass to form a primary film, the viscosity of the polyamic acid solution is 3200cP, and the primary film thickness is about 0.5mm.
[0070] (3) Use a spin coating device to rotate at a speed of 600r / min for 10s, and then rotate at a speed of 1000r / min for 25s to adjust the centrifugal thickness.
[0071] (4) The primary film and the carrier substrate adjusted by centrifugal thickening are sent as a whole into an oven with an inert gas argon atmosphere to solidify the primary film of polyamic acid to form a film. The temperature control process of the oven is as follows: heat preservation at 80°C for 30 minutes, heat preservation at 200°C for 30 minutes, heat preservation at 3...
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