Ceramic slice and preparation method thereof
A ceramic sheet and formula technology, applied in the field of ceramics, can solve the problems of easy breakage, short life, easy loss, etc., and achieve the effect of not easy to break, long life and small loss
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[0058] Such as figure 1 As shown, the invention provides a kind of preparation method of ceramic sheet, comprising:
[0059] S101, pre-pressing the pretreated powder to obtain a semi-finished product.
[0060] During the pre-press molding process of the pretreated powder, the pre-press molding pressure is 20-200T.
[0061] Preferably, the pressure of the pre-press forming is 38~60T.
[0062] More preferably, the pre-pressing pressure is 40T, 45T, 50T or 55T.
[0063] S102. Perform low-temperature heat treatment on the pre-pressed semi-finished product, wherein the temperature of the low-temperature heat treatment is 500-1100° C.
[0064] Preferably, the temperature of the low temperature heat treatment is 500°C to 1000°C.
[0065] S103, performing hot-press vibration sintering on the semi-finished product that has undergone low-temperature heat treatment, wherein the sintering temperature of the hot-press vibration is 1300-1700° C., and the pressure is 4-50 MPa.
[0066] ...
Embodiment 1
[0110] Mix 94% zirconia, 5% yttrium oxide, and 1% lanthanum oxide, add an adhesive polyvinyl alcohol aqueous solution for mixing and granulation; carry out dry pressing molding by a press, and the dry pressing pressure is 40T to obtain a semi-finished product; carry out at 800°C Low temperature heat treatment; then vibratory hot pressing sintering, the sintering temperature is 1470°C, and the pressure is 30MPa; finally, the vibratory hot pressing product is polished to obtain a zirconia ceramic sheet with a finished thickness of 0.3mm.
Embodiment 2
[0112] Mix 92% zirconia, 6% yttrium oxide, 1% cerium oxide and 1% praseodymium oxide, add an adhesive polyvinyl alcohol aqueous solution for mixing and granulation; perform dry pressing on a press with a dry pressing pressure of 45T to obtain a semi-finished product; Low temperature heat treatment at 600°C; then vibration hot pressing sintering, the sintering temperature is 1570°C, the pressure is 40MPa; finally, the vibration hot pressing product is polished to obtain a finished zirconia ceramic sheet with a thickness of 0.2mm.
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