A kind of building thermal insulation airgel material and preparation method thereof
A technology of building thermal insulation and airgel, which is applied in the field of building thermal insulation materials, can solve the problems of low strength, high cost, and complicated preparation process of airgel, and achieve the effects of good strength, high porosity, and simple production process
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0032] 1) Add 60 parts by weight of methyl orthosilicate and 20 parts by weight of ethylene glycol into the container and stir for 10 minutes, add 10 parts by weight of methyltriethoxysilane, add 10 parts of water, stir for 3 minutes, add hydrochloric acid Adjust the pH of the solution to 5, set the oil temperature in the container to 100°C and continue to stir and hydrolyze for 60 minutes to obtain a silica sol;
[0033]2) Grinding and modifying 80 parts of polyvinyl alcohol 1788, 10 parts of glycerin, 2 parts of polyethylene glycol-2000, and 1 part of borax to obtain polyvinyl alcohol hot melt adhesive powder;
[0034] 3) Add 10 parts by weight of polyvinyl alcohol hot melt adhesive powder and 2 parts of ethylene glycol (dioctyl pyrophosphate) titanium to 88 parts of silica sol solution, add triethanolamine to adjust the pH value to 10, stir evenly, and The polyvinyl alcohol hot melt adhesive powder is evenly dispersed in the wet gel, and then placed in a closed aging tank f...
Embodiment 2
[0040] 1) Add 55 parts by weight of tetraethyl orthosilicate and 20 parts by weight of ethylene glycol into the container and stir for 10 minutes, add 10 parts by weight of methyltriethoxysilane, add 15 parts of water, stir for 3 minutes, add hydrochloric acid Adjust the pH of the solution to 5, set the oil temperature in the container to 100°C and continue to stir and hydrolyze for 50 minutes to obtain a silica sol;
[0041] 2) Grinding and modifying 90 parts of polyvinyl alcohol 1788, 5 parts of glycerin, 2 parts of polyethylene glycol-2000, and 3 parts of succinic acid to obtain polyvinyl alcohol hot melt adhesive powder;
[0042] 3) Add 25 parts of polyvinyl alcohol hot melt adhesive powder and 2 parts of isopropoxytri(dioctyl pyrophosphate)titanium to 73 parts of silica sol solution, add triethanolamine to adjust the pH value to 10, stir evenly, and The polyvinyl alcohol hot melt adhesive powder is evenly dispersed in the wet gel, and then placed in a closed aging tank fo...
Embodiment 3
[0049] 1) Add 50 parts by weight of tetraethyl orthosilicate and 25 parts by weight of ethylene glycol into the container and stir for 5 minutes, add 5 parts by weight of methyltriethoxysilane, add 10 parts of water, stir for 3 minutes, add hydrochloric acid Adjust the pH of the solution to 5, set the oil temperature in the container to 100°C and continue to stir and hydrolyze for 30 minutes to obtain a silica sol;
[0050] 2) 85 parts of polyvinyl alcohol 1788, 8 parts of glycerin, 4 parts of polyethylene glycol-2000, and 3 parts of adipic acid were modified by grinding to obtain polyvinyl alcohol hot melt adhesive powder;
[0051] 3) Add 20 parts of polyvinyl alcohol hot melt adhesive powder and 2 parts of isopropoxytri(dioctyl pyrophosphate)titanium to 78 parts of silica sol solution, add triethanolamine to adjust the pH value to 9, stir evenly, and The polyvinyl alcohol hot melt adhesive powder is evenly dispersed in the wet gel, and then placed in a closed aging tank for ...
PUM
Property | Measurement | Unit |
---|---|---|
specific surface area | aaaaa | aaaaa |
diameter | aaaaa | aaaaa |
porosity | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com