A composite material for artificial teeth and its preparation method and application
A technology of artificial teeth and composite materials, applied in dental preparations, dentistry, dental prosthesis, etc., can solve the problem of poor mechanical properties of polymethyl methacrylate, restrictions on the popularization and application of polymethacrylate, difficulty in achieving biological fusion, etc. problem, to achieve the effect of strong wear resistance, meet the requirements of personalized production, and strong mechanical properties
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[0048] In a preferred embodiment of the present invention, the method for selective laser sintering of artificial teeth includes the following steps: raw material, powder preparation method and material molding method. The raw materials include polymethyl methacrylate, hydroxyapatite nanoparticles, emulsifier, microcrystalline wax and paraffin wax. The preparation method of the powder comprises the following steps: firstly adopting the wax emulsification method to modify the lipophilicity of the hydroxyapatite nanoparticles; Methyl ester powder material. The material forming method adopts a selective laser sintering method to form polymethyl methacrylate powder.
[0049] In a preferred embodiment of the present invention, the powder preparation method specifically includes the following steps:
[0050] Step (1) preparation of wax emulsion: adding emulsifier into water and stirring, adding microcrystalline wax and paraffin and heating to make wax emulsion;
[0051] Step (2) ...
Embodiment l
[0057] A kind of composite material for artificial tooth, the formula of its raw material is as follows:
[0058] Polymethyl methacrylate (120-500 mesh): 74 parts
[0059] Hydroxyapatite: 6 parts
[0060] Sodium lauryl sulfate: 10 parts
[0061] Microcrystalline wax and paraffin wax mixture: 10 parts (mass ratio is 5:10)
[0062] Preparation method: Add sodium lauryl sulfate to water and stir, then add a mixture of microcrystalline wax and paraffin wax and heat to 80°C for 60 minutes to make a wax emulsion. Then, the hydroxyapatite was prepared into an aqueous solution with a mass concentration of 5%, mixed with the wax emulsion, homogenized by a high-pressure homogenizer, then dried and ground at 105°C to obtain hydroxyapatite with surface lipophilicity. Finally, the prepared hydroxyapatite with good surface lipophilicity was added to the completely melted polymethyl methacrylate, and stirred for 30 minutes while heating to obtain a polymethyl methacrylate / hydroxyapatite c...
Embodiment 2
[0069] A kind of composite material for artificial tooth, the formula of its raw material is as follows:
[0070] Polymethyl methacrylate (120-500 mesh): 65 parts
[0071] Hydroxyapatite: 6 parts
[0072] Mixture of sodium lauryl sulfate and Span 60: 15 parts (mass ratio 7:10)
[0073] Microcrystalline wax and paraffin wax mixture: 14 parts (mass ratio is 8:10)
[0074] Preparation method: Add sodium lauryl sulfate into water and stir, then add a mixture of microcrystalline wax and paraffin wax and heat to 100°C for 30 minutes to make a wax emulsion. Then, the hydroxyapatite was prepared into an aqueous solution with a mass concentration of 7%, mixed with the wax emulsion, homogenized with a high-pressure homogenizer, then dried and ground at 105°C to obtain hydroxyapatite with surface lipophilicity. Finally, the prepared hydroxyapatite with good surface lipophilicity was added to the completely melted polymethyl methacrylate, and stirred for 30 minutes while heating to obt...
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