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A composite material for artificial teeth and its preparation method and application

A technology of artificial teeth and composite materials, applied in dental preparations, dentistry, dental prosthesis, etc., can solve the problem of poor mechanical properties of polymethyl methacrylate, restrictions on the popularization and application of polymethacrylate, difficulty in achieving biological fusion, etc. problem, to achieve the effect of strong wear resistance, meet the requirements of personalized production, and strong mechanical properties

Active Publication Date: 2015-10-21
INST OF CHEM CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the large differences in composition and structure with human bone tissue, the bone tissue repair process after implantation in the gums is basically a passive "filling" process, and the biocompatibility of the material is poor, making it difficult to achieve true "filling". "Biological fusion", even non-healing or loosening after implantation, and the mechanical properties of polymethyl methacrylate are also poor, making artificial tooth bases easy to crack, which seriously restricts the promotion of polymethyl methacrylate in dental clinics application
[0003] In addition, traditional dental implant technology is a complicated operation that requires a sterile environment in the operating room. After the tooth is extracted, the patient has to wait 3 months for the alveolar bone to heal before implanting a vertebral columnar bone on the alveolar bone. Alloy, that is, threaded nails, to replace the roots of the original real teeth, and wait for another 2 to 3 months before installing a false crown on the threaded screws. Once there is a gap between the artificial crown and the alloy root, bacteria will easily enter the human body , causing discomfort to the patient, and the whole process took about half a year, during which the patient had to come to the hospital three or four times

Method used

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preparation example Construction

[0048] In a preferred embodiment of the present invention, the method for selective laser sintering of artificial teeth includes the following steps: raw material, powder preparation method and material molding method. The raw materials include polymethyl methacrylate, hydroxyapatite nanoparticles, emulsifier, microcrystalline wax and paraffin wax. The preparation method of the powder comprises the following steps: firstly adopting the wax emulsification method to modify the lipophilicity of the hydroxyapatite nanoparticles; Methyl ester powder material. The material forming method adopts a selective laser sintering method to form polymethyl methacrylate powder.

[0049] In a preferred embodiment of the present invention, the powder preparation method specifically includes the following steps:

[0050] Step (1) preparation of wax emulsion: adding emulsifier into water and stirring, adding microcrystalline wax and paraffin and heating to make wax emulsion;

[0051] Step (2) ...

Embodiment l

[0057] A kind of composite material for artificial tooth, the formula of its raw material is as follows:

[0058] Polymethyl methacrylate (120-500 mesh): 74 parts

[0059] Hydroxyapatite: 6 parts

[0060] Sodium lauryl sulfate: 10 parts

[0061] Microcrystalline wax and paraffin wax mixture: 10 parts (mass ratio is 5:10)

[0062] Preparation method: Add sodium lauryl sulfate to water and stir, then add a mixture of microcrystalline wax and paraffin wax and heat to 80°C for 60 minutes to make a wax emulsion. Then, the hydroxyapatite was prepared into an aqueous solution with a mass concentration of 5%, mixed with the wax emulsion, homogenized by a high-pressure homogenizer, then dried and ground at 105°C to obtain hydroxyapatite with surface lipophilicity. Finally, the prepared hydroxyapatite with good surface lipophilicity was added to the completely melted polymethyl methacrylate, and stirred for 30 minutes while heating to obtain a polymethyl methacrylate / hydroxyapatite c...

Embodiment 2

[0069] A kind of composite material for artificial tooth, the formula of its raw material is as follows:

[0070] Polymethyl methacrylate (120-500 mesh): 65 parts

[0071] Hydroxyapatite: 6 parts

[0072] Mixture of sodium lauryl sulfate and Span 60: 15 parts (mass ratio 7:10)

[0073] Microcrystalline wax and paraffin wax mixture: 14 parts (mass ratio is 8:10)

[0074] Preparation method: Add sodium lauryl sulfate into water and stir, then add a mixture of microcrystalline wax and paraffin wax and heat to 100°C for 30 minutes to make a wax emulsion. Then, the hydroxyapatite was prepared into an aqueous solution with a mass concentration of 7%, mixed with the wax emulsion, homogenized with a high-pressure homogenizer, then dried and ground at 105°C to obtain hydroxyapatite with surface lipophilicity. Finally, the prepared hydroxyapatite with good surface lipophilicity was added to the completely melted polymethyl methacrylate, and stirred for 30 minutes while heating to obt...

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Abstract

The invention discloses a composite material for artificial teeth and a selective laser sinter molding method and an application thereof. The method includes raw materials, a powder preparation method and a material molding method. The raw materials contain polymethyl methacrylate, hydroxyapatite nano-particles, an emulsifier, microcrystalline wax and paraffin. The powder preparation method comprises the following steps: firstly carrying out lipophilic modification on the hydroxyapatite nano-particles by a wax emulsification method and then preparing a polymethacrylate powder material doped with the hydroxyapatite nano-particles by hot-melting mechanical agitation and crushing ball milling. According to the molding method, a polymethacrylate powder is molded by a selective laser sintering technology. By the adoption of the artificial teeth dedicated composite material with a composite bioactivity, the problem that traditional artificial teeth have insufficient mechanical strength and poor compatibility can be solved effectively. In addition, as the selective laser sinter molding technology is provided, preparation time of artificial teeth is shortened greatly, teeth replacement cycle is minimized for patients, and requirements of doctors and patients on artificial teeth are met.

Description

technical field [0001] The invention relates to a composite material for artificial teeth and its preparation method and use, in particular to a composite material for artificial teeth and its selective laser sintering preparation method and use. Background technique [0002] At present, the most clinically used artificial tooth material is polymethyl methacrylate, which is favored by doctors and doctors because of its advantages of corrosion resistance, strong resistance to fragmentation, strong designability, low cost, and durability. Patients welcome. However, due to the large difference in composition and structure with human bone tissue, the bone tissue repair process after implantation in the gums is basically a passive "filling" process, and the biocompatibility of the material is poor, making it difficult to achieve a real " "Biological fusion", even non-healing or loosening after implantation, and the mechanical properties of polymethyl methacrylate are also poor, ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K6/083A61K6/033A61K6/838
Inventor 王春燕沈衡朱唐赵宁徐坚孙文华董金勇李春成符文鑫林学春马永梅
Owner INST OF CHEM CHINESE ACAD OF SCI
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