A kind of nanocrystalline complex-phase rare earth-transition group metal-b permanent magnet alloy magnetic powder and its manufacturing method
A technology of transition group metals and permanent magnet alloys, applied in the direction of magnetic materials, magnetic objects, inorganic materials, etc.
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Embodiment 1
[0027] .The preparation method and technological process of the quick-quenching nanocrystalline composite phase rare earth (RE)-transition metal (TM)-B permanent magnetic alloy magnetic powder are as follows:
[0028] 1. Alloying
[0029] Using Nd, Fe, Pt and BFe (containing B19wt%) with a purity of 99.9% as raw materials, according to the alloy composition ratio: Nd: 21wt%, .Pt: 7.1wt%, BFe alloy (containing B19wt%): 4.1wt% , Weigh the ingredients with the remaining Fe, then evacuate, and under the protection of argon, use an intermediate frequency induction furnace to melt into a rare earth (RE)-transition metal (TM)-B master alloy ingot.
[0030] 2.Quick quenching belt, milling
[0031] Put the rare earth (RE)-transition group metal (TM)-B master alloy ingot into a quartz tube with a small hole at the bottom, vacuum it, and melt it by medium frequency induction under the protection of argon. The molten alloy is sprayed on a water-cooled metal molybdenum roller that rotate...
Embodiment 2
[0036]Using Nd, Fe, Pt and BFe (containing B19wt%) with a purity of 99.9% as raw materials, according to the alloy composition ratio: Nd: 18.5wt%, .Pt: 6.2wt%, BFe alloy (containing B19wt%): 3.6wt %, surplus Fe weighs batching, and processing condition is with embodiment one, and the magnetic property that obtains magnetic powder is:
[0037] Br: 1.16kGs Hci: 5.83kOe(BH)max: 14.17MGOe.
Embodiment 3
[0039] With a purity of 99.9% Nd, Fe, Pt and BFe (containing B19wt%) as raw materials, according to the alloy composition ratio: Nd: 20wt%, .Pt: 13.5wt%, BFe alloy (containing B19wt%): 4wt%, Surplus Fe weighs batching, and processing condition is the same as embodiment one, and the magnetic property that obtains magnetic powder is:
[0040] Br: 8.79kGs Hci: 7.72kOe(BH)max: 11.78MGOe.
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