Homopolymer anti-scaling agent synthesis process capable of controlling reaction temperature
A technology of reaction temperature and synthesis process, which is applied in the field of homopolymer antifouling agent synthesis technology, can solve the problems of affecting the molecular weight of the polymer, affecting the antifouling performance of the polymer, and the great influence of the reaction temperature on the polymerization rate. Excellent scaling performance, low cost and short time effect
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[0027] A kind of homopolymer antiscaling agent synthetic process that the present invention relates to controlled reaction temperature, comprises steps:
[0028] (a) First, prepare the reaction monomers required for the synthesis process;
[0029] (b) Then, take a certain amount of reaction monomer and place it in a reaction container, and add a solvent and stir evenly;
[0030] (c) adding initiator in reaction vessel;
[0031] (d) adjusting the pH value of the reaction system;
[0032] (e) Place the reaction vessel in a water bath at 73°C to 78°C, and carry out stirring reaction at a certain speed;
[0033] (f) filtering the reaction product mixture after cooling;
[0034] (g) distilling the filtered liquid, drying after separation to obtain the target product.
[0035] The reaction vessel is a beaker.
[0036] Distillation under reduced pressure was carried out by rotary evaporator.
[0037] The solvent is distilled water.
[0038] The initiator is ammonium persulfate...
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