Method for preparing tantalum (Ta)-doped wolfram (W)-oxide adsorption nano-material
A nano-tungsten oxide, adsorption material technology, applied in chemical instruments and methods, radioactive purification, other chemical processes, etc., can solve the problems of difficult introduction of transition metal ions, difficult control and improvement of pore channels and pore types, and easy removal, etc. Achieve stable physical and chemical properties, smooth pores, and maintain stability
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Embodiment 1
[0042] Weigh 7 parts of sodium tungstate (NaWO 4 2H 2 O) Place in a polytetrafluoroethylene reactor, add 7 parts of double distilled water, stir to make it fully dissolved, add 7 parts of tantalum pentachloride ethanol solution with a concentration of 0.05mol / L, and make the solution Ta / W molar ratio 0.01 Continue stirring to make it fully mixed, then add 7 parts of 3mol / L hydrochloric acid solution and 7 parts of 0.5mol / L ammonium sulfate solution, stir for 0.5h, seal the polytetrafluoroethylene reaction kettle, place it in a programmed oven, and set the temperature to rise and a cooling rate of 1 degree 170 Hydrothermal treatment for 48h. Take out the reactor and cool to room temperature. Wash the reaction products with distilled water until neutral, and then place them at -40 Freeze drying in a freeze dryer to obtain tantalum doped hex-WO3 nanomaterials.
Embodiment 2
[0044] Weigh 10 parts of sodium tungstate (NaWO 4 2H 2 O) Put it in a polytetrafluoroethylene reactor, add 10 parts of secondary distillation, stir to make it fully dissolved, add 10 parts of tantalum pentachloride ethanol solution with a concentration of 0.05mol / L, and make the mole of Ta / W in the solution The ratio is 0.18, continue stirring to make it fully mixed, then add 10 parts of 2mol / L hydrochloric acid solution and 10 parts of 0.4mol / L ammonium sulfate solution, stir for 1h, seal the polytetrafluoroethylene reaction kettle, and place it in a programmed oven. Set the heating and cooling rate to 1°C / min, and conduct hydrothermal treatment at 200°C for 24 hours. After the reaction is completed, take out the reactor and cool to room temperature. Wash the reaction products with distilled water until neutral, and then freeze at -40°C Freeze drying in a dryer to obtain tantalum doped hex-WO 3 nanomaterials.
Embodiment 3
[0046] Weigh 8 parts of sodium tungstate (NaWO 4 2H 2 O) Put it in a polytetrafluoroethylene reaction kettle, add 8 parts of double distilled water, stir to make it fully dissolved, add 8 parts of tantalum pentachloride ethanol solution with a concentration of 0.05mol / L, and make the mole of Ta / W in the solution The ratio is 0.05, continue to stir to make it fully mixed, then add 8 parts of 3mol / L hydrochloric acid solution and 0.5mol L -1 8 parts of ammonium sulfate solution, stirred for 0.8h, sealed the polytetrafluoroethylene reaction kettle, placed in a programmed oven, set the heating and cooling rate to 1°C / min, and hydrothermally treated at a temperature of 175°C for 40h. After the reaction was completed, the reaction kettle was taken out , cooled to room temperature. The reaction products were washed with distilled water until neutral, and then placed in a freeze-dryer at a temperature of -40°C to obtain tantalum-doped hex-WO 3 nanomaterials.
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