Method for preparing furfural compounds from biomass
A technology of biomass and compounds, applied in the direction of organic chemistry, etc., can solve the problems of catalysts that cannot be recycled and reused, high requirements for reaction equipment, and high cost, and achieve the effects of low cost, low equipment corrosion, and improved service life
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Embodiment 1-8
[0017] Catalyst preparation by ion exchange method: Weigh a certain mass of molecular sieve or clay minerals and metal chlorides, nitrates, acetates or bromides, and then add them to a beaker containing 300mL of water, and carry out ion exchange at a specific temperature After a period of time, the catalyst in the beaker was taken out, filtered and washed, and dried overnight at a temperature of 100°C.
[0018] In eight reactors of the same type, 10 mL of an aqueous solution of methyl isobutyl ketone and saturated potassium chloride with a volume ratio of 7: 3 was added, then 0.5 g of glucose was added, and 0.1 g of the catalysts of Examples 1-8 were added respectively. , tighten the screws of the reactor, fill with nitrogen protective gas, place in eight different heating mantles respectively, raise the heating mantles to 160°C, keep the temperature constant, stir, and stop the reaction after 3 hours of reaction. The reaction system was cooled to room temperature, and the cat...
Embodiment 9-17
[0022] In nine reactors of the same type, add 10 mL of saturated aqueous solution of methyl isobutyl ketone and different inorganic salts with a volume ratio of 7:3, then add 0.5 g of glucose and 0.1 g of the catalyst of Example 5 respectively, and tighten the reaction The screw of the device was filled with nitrogen protective gas, and placed in nine different heating mantles respectively, and the heating mantles were respectively raised to 160 ° C, kept at constant temperature, stirred, and the reaction was stopped after 3 hours of reaction. The reaction system was cooled to room temperature, and the catalyst was separated by centrifugation. The reaction solution was detected by high performance liquid chromatography, and the results obtained from the reaction under different saturated inorganic salt solutions are shown in Table 2.
[0023] The yield of 5-hydroxymethylfurfural under different saturated inorganic salt solutions of table 2
[0024] Example serial num...
Embodiment 18-27
[0026]In ten reactors of the same model, add different organic solvents and saturated potassium chloride solution with a volume ratio of 7:3, then add 0.5g of glucose and 0.1g of the catalyst of Example 5 respectively, tighten the screws of the reactors, and be full of nitrogen Protective gas was placed in ten different heating mantles respectively, and the heating mantles were raised to 160° C., kept at constant temperature, stirred, and reacted for 3 hours to stop the reaction. The reaction system was cooled to room temperature, and the catalyst was separated by centrifugation. The reaction solution was detected by high-performance liquid chromatography, and the results obtained in different organic solvents are shown in Table 3.
[0027] The yield of 5-hydroxymethylfurfural under different organic solvents of table 3
[0028] Example serial number
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