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Method of acquiring tri-modal microstructure in near-alpha titanium alloy through furnace cooling

A titanium alloy and microstructure technology, which is applied in the field of heat treatment for obtaining three-state microstructures by furnace cooling, can solve the problems of narrow temperature range, inconvenient forging temperature, and small secondary flake α thickness.

Inactive Publication Date: 2013-07-17
NORTHWESTERN POLYTECHNICAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] In order to overcome the problems in the prior art that the temperature range is narrow, it is not convenient to control the forging temperature, and the limitation of the initial structure is a two-state structure, and the thickness of the secondary lamellar α in the obtained three-state structure is too small problem, the present invention proposes a method for obtaining a triple-state structure in a near-alpha titanium alloy

Method used

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  • Method of acquiring tri-modal microstructure in near-alpha titanium alloy through furnace cooling
  • Method of acquiring tri-modal microstructure in near-alpha titanium alloy through furnace cooling
  • Method of acquiring tri-modal microstructure in near-alpha titanium alloy through furnace cooling

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Embodiment 1

[0015] This embodiment is a method for obtaining a three-state structure by furnace cooling in a near-alpha titanium alloy. The sample used is a TA15 titanium alloy, and the shape of the sample is cylindrical. The specification of the sample is Φ10*15mm; TA15 titanium alloy is Ti-6Al-2Zr-1Mo-1V. The β transformation point of TA15 titanium alloy is 990°C, and the initial structure is equiaxed.

[0016] The specific implementation steps of this embodiment are:

[0017] Step 1, heat preservation and water cooling near the β temperature.

[0018] The resistance furnace is heated to the near β temperature of the TA15 titanium alloy, that is, the temperature range is 10-20°C lower than the β transformation point. In this embodiment, the temperature of the resistance furnace is 975°C, which is 15°C lower than the β temperature of the TA15 titanium alloy. When the temperature of the resistance furnace reaches 975°C, put the cylindrical sample into the resistance furnace. Heat the r...

Embodiment 2

[0024] This embodiment is a method for obtaining a three-state structure by furnace cooling in a near-α titanium alloy. The sample used is a TA15 titanium alloy, and the shape of the sample is cylindrical. The specification of the sample is Φ210*300mm; TA15 titanium alloy is Ti-6Al-2Zr-1Mo-1V. The β transformation point of TA15 titanium alloy is 990°C, and the initial structure is a two-state structure.

[0025] The specific implementation steps of this embodiment are:

[0026] Step 1, heat treatment near β temperature. The resistance furnace is heated to the near β temperature of the TA15 titanium alloy, that is, the temperature range is 10-20°C lower than the β transformation point. In this embodiment, the temperature of the resistance furnace is 970°C, which is 20°C lower than the β temperature of the TA15 titanium alloy. When the temperature of the resistance furnace reaches 970°C, put the cylindrical sample into the resistance furnace. Heat the resistance furnace to 97...

Embodiment 3

[0030] This embodiment is a method for obtaining a three-state structure by furnace cooling in a near-α titanium alloy. The sample used is a TA11 titanium alloy, and the shape of the sample is cylindrical. The specification of the sample is Φ15*25mm; TA11 titanium alloy is Ti-8Al-1Mo-1V. The β transformation point of TA11 titanium alloy is 1040 ℃, and the initial structure is equiaxed.

[0031] The specific implementation steps of this embodiment are:

[0032] Step 1, heat treatment near β temperature. The resistance furnace is heated to the near β temperature of the TA11 titanium alloy, that is, the temperature range is 10-20°C lower than the β transformation point. In this embodiment, the temperature of the resistance furnace is 1020°C, which is 20°C lower than the β temperature of the TC4 titanium alloy. When the temperature of the resistance furnace reaches 1020°C, put the cylindrical sample into the resistance furnace. Heat the resistance furnace to 1020°C and start he...

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Abstract

The invention provides a method of acquiring a tri-modal microstructure in a near-alpha titanium alloy through furnace cooling. According to the method, near-beta temperature heat-insulating water cooling and two-phase region temperature heat-insulating furnace cooling and air cooling are carried out so as to obtain the near-alpha titanium alloy with the tri-modal microstructure; 10 to 20% of an equiaxial primary alpha phase can be retained in a titanium alloy microstructure through the near-beta temperature heat-insulating water cooling, with the balance being martensite; and a tri-modal microstructure titanium alloy consisting of equiaxial alpha, sliver alpha and a beta transformation microstructure is finally formed through the two-phase region temperature heat-insulating furnace cooling and air cooling. The method provided in the invention needs no near-beta thermal deformation and does not generate non-uniform deformation heat effects, temperature can be easily controlled, and special pretreatment does not need to be carried out on the equiaxed-structure near-alpha titanium alloy so as to acquire a duplex microstructure. The thickness value of secondary flake alpha in the invention is in a great adjustable range; the method is simple and easy to implement, has a wide application scope and is applicable to heat treatment of near-alpha titanium alloy parts manufactured by using methods like rolling, extrusion and machining molding.

Description

technical field [0001] The invention relates to the technical field of thermal processing of titanium alloys, in particular to a heat treatment method for obtaining a triple-state structure by using furnace cooling in near-alpha titanium alloys with equiaxed or double-state structures. Background technique [0002] Near-α titanium alloys have better thermal stability and weldability than α+β-type titanium alloys, and better pressure processing performance than α-titanium alloys. They are usually used in key load-bearing structural parts in aviation, aerospace and other fields. These components are served in harsh environments, requiring not only high precision, but also high performance and high reliability, that is to say, good room temperature strength plasticity, fracture toughness, fatigue performance, crack growth resistance and high temperature performance. The microstructure of titanium alloy determines the service performance. Equiaxed microstructure and lamellar mi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22F1/18
Inventor 孙志超杨合郭双双马超
Owner NORTHWESTERN POLYTECHNICAL UNIV
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