Method for preparing alumina by using power plant fly ash
A technology for power plant fly ash and alumina, applied in the field of non-ferrous metal metallurgy, can solve the problem of high alumina process cost, achieve the effects of high energy utilization rate, low production cost and simplified process steps
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Embodiment 1
[0016] Take 1,000 grams of fly ash, grind it to 100 μm, mix the fly ash with 2,600 ml of sulfuric acid with a mass percentage of 75%, and leach at 100°C for 1 hour; filter the fly ash leached by sulfuric acid to separate the remaining acid from the filter residue . Add 3000ml of water to the filter residue, boil and dissolve at 50°C for 30 minutes to dissolve the reactant, filter to remove the residue, and obtain an aluminum sulfate solution.
[0017] The aluminum sulfate solution was heated and concentrated to 1000ml, 5500ml of 15% hydrochloric acid was added, and then HCl gas was introduced to precipitate aluminum chloride crystals, which were filtered to obtain 1853 grams of aluminum chloride crystals.
[0018] use NH 3 1750ml of 25%wt ammonium hydroxide solution was reacted with aluminum chloride solution to obtain aluminum hydroxide precipitate and ammonium chloride solution. After filtration, aluminum hydroxide crystals are calcined at 1100°C to obtain Al 2 o 3 358.5...
Embodiment 2
[0021] Take 1,000 grams of fly ash, grind it to 125 μm, mix the fly ash with 6,000 ml of sulfuric acid with a mass percentage of 80%, and leach at 150°C for 1.5 hours; filter the fly ash leached by sulfuric acid to separate the residual acid from the filter residue . Add 3500ml of water to the filter residue, boil and dissolve at 60°C for 40 minutes to dissolve the reactant, filter to remove the residue, and obtain an aluminum sulfate solution.
[0022] Evaporate and crystallize the aluminum sulfate solution to obtain 2719 grams of Al 2 (SO4) 3 18H 2 O crystals, aluminum sulfate crystals are mixed with 4500ml of 32% hydrochloric acid, then feed HCl gas, separate out aluminum chloride crystals, filter to obtain 1916 grams of aluminum chloride crystals.
[0023] use NH 3 1750ml of 25%wt ammonium hydroxide solution was reacted with aluminum chloride solution to obtain aluminum hydroxide precipitate and ammonium chloride solution. After filtering, calcining aluminum hydroxide...
Embodiment 3
[0026] Take 1,000 grams of fly ash, grind it to 150 μm, mix the fly ash with 3,500 ml of sulfuric acid with a mass percentage of 90%, and leach at 200°C for 2 hours; filter the fly ash leached by sulfuric acid to separate the remaining acid from the filter residue . Add 4000ml of water to the filter residue, boil and dissolve at 70°C for 45 minutes to dissolve the reactant, filter to remove the residue, and obtain an aluminum sulfate solution.
[0027] The aluminum sulfate solution was heated and concentrated to 1000ml, 3500ml of 25% hydrochloric acid was added, and then HCl gas was introduced to precipitate aluminum chloride crystals, which were filtered to obtain 1911 grams of aluminum chloride crystals.
[0028] Take 400g of liquid ammonia, add aluminum chloride to 2500ml of water to dissolve, and mix the liquid ammonia with the aluminum chloride solution to obtain aluminum hydroxide precipitate and ammonium chloride solution. After filtration, the aluminum hydroxide cryst...
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