Coal-based environment-friendly solvent oil and preparation method thereof
An environmentally friendly solvent, coal-based technology, used in the petroleum industry, hydrocarbon oil treatment, hydrotreating processes, etc., can solve problems such as benzene content limitation and hematopoietic system diseases, and achieve good lubricity, low freezing point, and good performance. Effect
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example 1
[0034] A typical shale oil is selected as the raw material, and the properties of the shale oil raw material after dehydration and removal of mechanical impurities are shown in Table 1. The shale oil raw material is distilled to separate light oil and heavy oil, light oil The distillation cut point of heavy oil and heavy oil is 350°C. The heavy oil is operated continuously on a 0.1t / d continuous suspension bed hydrocracking test device. The adopted process conditions are: reaction temperature 420°C, reaction pressure 15MPa, volume space velocity 0.5h -1 , the volume ratio of hydrogen to oil is 1500, the catalyst is a composite multi-metal active component containing molybdenum and iron, and the particle diameter is less than 50 μm in powder form. The amount of catalyst added is to control the total amount of metal in the active component and the weight of the heavy oil raw material The ratio is 0.8:100. The suspended bed light oil fraction produced by continuous operation and...
example 2
[0041] A typical coal tar was selected as the raw material for the test. The properties of the coal tar raw material after dehydration and removal of mechanical impurities are shown in Table 3. The coal tar raw material was distilled to separate light oil and heavy oil. The heavy oil was separated at 0.1 The t / d continuous suspension bed hydrocracking test device operates continuously and adopts the following process conditions: reaction temperature 430°C, reaction pressure 16 MPa, volumetric space velocity 0.5 h -1 , the volume ratio of hydrogen to oil is 1500, the catalyst is a composite multi-metal active component containing molybdenum and iron, and the particle diameter is less than 50 μm. The ratio is 0.8:100. The suspended bed light oil fraction produced by continuous operation and the light oil separated from the coal tar raw material by distillation are mixed as the raw material for fixed bed hydrofining, and then hydrofining is carried out on a 3L / hr continuous hydro...
example 3
[0048] The test selects a typical dephenolized oil fraction as raw material, and the properties of the dephenolized oil raw material after dehydration and removal of acid-base residue pretreatment are shown in Table 5. The dephenolized oil raw material is used as a fixed bed hydrorefining raw material, and then the The hydrogenation refining is carried out on the continuous hydrogenation device of hr, and the hydrofinishing process conditions are: two fixed bed reactors connected in series, the reaction pressure is 12.0MPa, the reaction temperature is 350°C, and the space velocity is 1.0 h -1 , The volume ratio of hydrogen to oil is 800:1, and the catalyst is Ni-Mo series hydrogenation protecting agent and Ni-Mo-Wo series hydrofining catalyst. Hydrorefined coal tar hydrorefined oil is obtained.
[0049] The dephenolized oil obtained above is hydrotreated and refined, and then rectified, fractionated and cut to obtain 150-200°C fractions or 160-200°C fractions, etc., to obtain ...
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