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Device for measuring droplet contact angle and rolling angle under temperature control, humidity control and pressure control condition

A technology of contact angle and rolling angle, applied in the field of chemical measurement, can solve problems such as errors, image distortion results, limit the test range of contact angle and rolling angle, etc., and achieve high degree of automation, high test accuracy and good repeatability Effect

Inactive Publication Date: 2012-08-01
NANJING UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] (1). It can only be tested under normal pressure, which limits the test range of contact angle and rolling angle, and cannot obtain contact angle and rolling angle under variable pressure conditions.
[0006] (2). Under very low temperature conditions such as -20°C, even the outer surface of double-layer quartz glass will form serious water mist, and it is necessary to wipe the window with a cotton ball dipped in antifreeze The surface, the wiping process will block the camera lens image shooting, and the water mist left on the quartz glass surface will change the direction of the optical path, distorting the captured image and causing errors in the results
[0007] (3). The maximum speed of the high-speed camera used is only 420 frames per second, which cannot track the freezing process of water droplets on superhydrophobic surfaces in real time or the bouncing and viscoelastic processes of water droplets on superhydrophobic surfaces in real time.

Method used

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  • Device for measuring droplet contact angle and rolling angle under temperature control, humidity control and pressure control condition
  • Device for measuring droplet contact angle and rolling angle under temperature control, humidity control and pressure control condition
  • Device for measuring droplet contact angle and rolling angle under temperature control, humidity control and pressure control condition

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Example 1: The contact angle, rolling angle, advancing angle, receding angle and lagging angle of water droplets on a superhydrophobic surface under the conditions of 40°C, 60% relative humidity, and 0.5MPa pressure.

[0032] Fix the sample box on the rotating bracket. The rotating bracket is located between the light source and the high-speed camera lens. Place the sample to be tested in the center of the sample box. Adjust the position of the rotating bracket so that the LED cold light source, optical quartz glass , the high-speed camera (Phantom V12.0) are located on the same line, the LED cold light source illuminates the test drop through the optical quartz glass window, the high-speed camera system obtains the image data of the test drop through the optical quartz glass window, and the temperature The sensor, humidity sensor and pressure sensor are connected to the computer system, the stepper motor (Haydon Switch & Instrument INC.) is connected to the driver (Step...

example 2

[0034] Example 2: The contact angle and rolling angle of a water droplet on a glass surface at 0°C and a vacuum of 0.1kpa

[0035] Fix the sample box on the rotating bracket, the rotating bracket is located between the LED cold light source and the high-speed camera lens, place the sample to be tested in the center of the sample box, adjust the position of the rotating bracket so that the LED cold light source, optical quartz glass window, The sample surface and the high-speed camera are located on the same line. The LED cold light source illuminates the test droplet through the optical quartz glass window. It is connected to the computer system, the stepper motor is connected to the driver, the circulation pipeline in the sample box wall is connected to the temperature control system through the interface and the conduit, the vacuum pump is connected to the sample box, the anti-condensation exposed air port on the surface of the optical quartz glass is connected to the dry Th...

example 3

[0037] Example 3: At -10°C, 50% relative humidity, and normal pressure, high-speed tracking of the bouncing process of water droplets falling from a height of 0.5cm on a superhydrophobic surface with an inclination angle of 10°

[0038] Fix the sample box on the rotating bracket, the rotating bracket is located between the LED cold light source and the high-speed camera lens, place the sample to be tested in the center of the sample box, adjust the position of the rotating bracket so that the LED cold light source, optical quartz glass window, The sample surface and the high-speed camera are located on the same line. The LED cold light source illuminates the test drop through the optical quartz glass window. The high-speed camera system obtains the image data of the test drop through the window. The temperature sensor and humidity sensor installed on the sample box are connected to the computer system. Connection, the circulating pipeline in the wall of the sample box is connec...

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Abstract

The invention belongs to the technical field of chemical measurement and in particular relates to a device for measuring a droplet contact angle and a rolling angle under a temperature control, humidity control and pressure control condition. A temperature control system is used for accurately controlling the temperature in a specimen box within a range from -20 DEG C to +200 DEG C; a humidity control system is used for controlling the relative humidity range at 0-100%; a vacuum / pressure control system comprises a high pressure system and a vacuum system; the pressure control range is from 10-6 Pa to 8.5 MPa; an anti-fogging device is used for preventing the surface of a glass window from fogging; a high speed image pickup system is used for obtaining a testing droplet contour image; the image sampling speed can reach 1400 thousand frames per second; the highest resolution reaches 1280x800; image sampling data is transmitted to a computer system by a data wire; and the image is fitted by using software according to a Young-Laplace equation so as to the contact angle, rolling angle, advancing angle, backing angle and viscoelastic property of the droplet. The device provided by the invention has the advantages of high automatic degree, testing accuracy, good experiment result repeatability, suitability for a wide temperature range, broad humidity, high pressure and negative pressure system to measure the contact angle, rolling angle, advancing angle, backing angle and lag angle of the droplet.

Description

technical field [0001] The invention relates to a device for measuring droplet contact angle and rolling angle under the conditions of wide temperature range, wide humidity, high pressure and negative pressure, belonging to the technical field of chemical measurement. technical background [0002] Super-hydrophobic phenomena are widespread in nature. For example, the surface of lotus leaves has strong hydrophobicity and self-cleaning functions; the wings of butterflies, the feet of water striders, and the feathers of waterfowl all have super-hydrophobic properties. At present, through the research and imitation of natural plant leaves, a large number of bionic surfaces with excellent self-cleaning effects emerge in endlessly. If a deeper understanding of the mechanism of action of superhydrophobic surfaces can be obtained, it will undoubtedly have important guiding and practical value for the design and manufacture of new superhydrophobic and self-cleaning surfaces. The rol...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N13/00G05D27/02
Inventor 王庆军薛健朱林王媛怡丁国伟陈庆民
Owner NANJING UNIV
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