Azoxystrobin microcapsule suspending agent and preparation method thereof
A microcapsule suspending agent, azoxystrobin technology, applied in the directions of botanical equipment and methods, fungicides, biocides, etc., can solve the problem of large application concentration of azoxystrobin, no synergist added, and short duration of efficacy. and other problems, to achieve the effect of consolidating the control effect, prolonging the validity period of the drug effect, and easy to control the process.
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Embodiment 1
[0021] Example 1: 5% azoxystrobin microcapsule suspension.
[0022] Dissolve urea in formaldehyde, the weight ratio of urea and formaldehyde is 1:2, adjust the pH value to 8.5 with 10% NaOH solution, stir with a magnetic stirrer until clear, stir at a low speed at a temperature of 70°C, and keep warm React for 1 hour to generate viscous and transparent urea-formaldehyde resin, add deionized water equal to the total weight of urea and formaldehyde, and stir at a low speed to obtain a transparent urea-formaldehyde resin prepolymer aqueous solution.
[0023] At room temperature, dissolve 5% azoxystrobin in 15% xylene, add 2% Nongru 600# to fully emulsify, and stir at 1000 rpm at a temperature of 30°C to fully disperse it.
[0024] Add an appropriate amount of urea-formaldehyde resin prepolymer aqueous solution to the above-mentioned azoxystrobin mixture solution under stirring at 1000 rpm, stir for 15 minutes to form a stable emulsion, then reduce the stirring rate to 500 rpm, a...
Embodiment 2
[0025] Example 2: 8% azoxystrobin microcapsule suspension.
[0026] Dissolve urea in formaldehyde, the weight ratio of urea and formaldehyde is 1:2.5, adjust the pH value to 8.5 with 10% NaOH solution, stir with a magnetic stirrer until clear, and stir at a low speed at a temperature of 70°C, keep warm After reacting for 1.5 hours, a viscous and transparent urea-formaldehyde resin is formed, adding deionized water equal to the total weight of urea and formaldehyde, and stirring at a low speed to obtain a transparent urea-formaldehyde resin prepolymer aqueous solution.
[0027] At room temperature, dissolve 8% azoxystrobin in 15% dimethylformamide, add 7% agricultural milk 700# to fully emulsify, and stir at 1500 rpm at a temperature of 30°C to make it fully dispersion.
[0028] Add an appropriate amount of urea-formaldehyde resin prepolymer aqueous solution to the above-mentioned azoxystrobin mixture solution stirred at 1500 rpm, stir for 15 minutes to form a stable emulsio...
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