Polyurea calcium acetate lubricating grease and preparation method thereof
A technology of lubricating grease and calcium acetate, applied in lubricating compositions, petroleum industry, etc., can solve the problems of short service life, poor colloidal stability of lubricating grease, thinning and loss of lubricating grease, etc., and achieve good colloidal stability and good colloidal stability The effect of high resistance and good water resistance
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Embodiment 1
[0020] In the reaction vessel, add 180.5 kg of 120BS and 30 kg of MDI, stir and heat to raise the temperature to 40-50°C, add 64.6 kg of melted stearylamine, heat and raise the temperature to 100-110°C, stir and react at a constant temperature for 10 minutes. Add 395 kg of synthetic calcium sulfonate with a total alkali value of 300 mgKOH / g into the reaction vessel, and slowly add 120 kg of glacial acetic acid under stirring. After the addition, stir and heat to 150-160°C, add 10 kg of diphenylamine antioxidant and 1 kg of benzotriazole anti-corrosion additive, stir and mix for 5 minutes, and stop heating. Add 198.9 kg of 120BS with stirring and cool to 80-100°C, homogenize and degas to obtain the product. The properties of the product obtained in this example are shown in Table 1.
Embodiment 2
[0022] In the reaction vessel, add 180.5 kg of HVI500 and 30 kg of MDI, stir and heat to raise the temperature to 40-50°C, add 64.6 kg of molten octadecylamine, heat and raise the temperature to 100-110°C, stir and react at a constant temperature for 10 minutes. Add 437 kg of calcium petroleum sulfonate with a total alkali value of 270 mgKOH / g into the reaction vessel, and slowly add 120 kg of glacial acetic acid under stirring. After the addition, stir and raise the temperature to 150-160°C, add 2 kg of diisooctyl diphenylamine antioxidant and 3 kg of T561, stir and mix for 5 minutes, and stop heating. Add 162.9 kg of 150BS with stirring and cool to 80-100°C, homogenize and degas to obtain the product. The properties of the product obtained in this example are shown in Table 1.
Embodiment 3
[0024] In the reaction vessel, add 200 kg of No. 100 mechanical oil and 40 kg of MDI, stir and heat up to 40-50℃, add 43 kg of melted octadecylamine and 19.8 kg of cyclohexylamine, heat up to 100-110℃, stir React at constant temperature for 10 minutes. Add 245 kg of calcium petroleum sulfonate with a total alkali value of 400 mgKOH / g into the reaction vessel, and slowly add 100 kg of glacial acetic acid under stirring. After the addition, stir and heat to 150-160°C, add 1 kg of diisooctyl diphenylamine antioxidant, 3 kg of diphenylamine and 0.5 kg of T551, stir and mix for 5 minutes, and stop heating. Add 347.7 kg of 150BS with stirring and cool to 80-100°C, homogenize and degas to obtain the product. The properties of the product obtained in this example are shown in Table 1.
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