Xingnaojing solid medicinal composition and preparation method thereof
A technology of Xingnaojing and its composition, which is applied in the field of medicine, can solve the problems of insufficient utilization of active ingredients, increase of toxic substances, large energy consumption, etc., and achieve the effects of improving bioavailability, taking conveniently, and fully extracting
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Embodiment 1
[0047] Prescription: gardenia 3000g, turmeric 3000g, artificial musk 750g, borneol 100g
[0048] 1. Take gardenia and turmeric decoction pieces, grind them into coarse powder respectively, mix them and put them into a multi-energy extraction tank, add 8 times the amount of water, and extract the volatile oil. After 4 hours, 9.65 g of volatile oil was collected.
[0049] 2. After the extraction of volatile oil, the medicinal liquid is first filtered and sucked into the storage tank. Add 10 times the amount of water (5 times the amount, 5 times the amount) to the dregs of the medicine, decoct and extract twice, each time for 1.5 hours, and inhale the above-mentioned extract after the initial filtration. In the storage tank, the medicinal liquid is centrifuged by a GQ-105 tubular separator, and after the supernatant is removed from the centrifuged liquid, it is adsorbed on a D4006 macroporous resin (40 mesh) column, and the flow rate is adjusted to 50ml / min (taking a 120*15cm col...
Embodiment 2
[0057] Prescription: gardenia 6000g, turmeric 6000g, artificial musk 1500g, borneol 200g
[0058] 1. Take gardenia and turmeric decoction pieces, grind them into coarse powder respectively, mix them and put them into a multi-energy extraction tank, add 8 times the amount of water, and extract the volatile oil. After 5 hours, 19.02 g of volatile oil was collected.
[0059] 2. After the extraction of volatile oil, the medicinal liquid is first filtered and sucked into the storage tank. Add 9 times the amount of water (5 times, 4 times) to the medicinal residue, and decoct and extract twice, each time for 1.5 hours. The extract is first filtered and sucked into the above-mentioned In the storage tank, the medicinal liquid is centrifuged by a GQ-105 tubular separator, and after the supernatant is removed from the centrifuged liquid, it is adsorbed on a D4006 macroporous resin (60 mesh) column, and the flow rate is adjusted to 100ml / min (taking a 160*18cm column as an example ), w...
Embodiment 3
[0067] Prescription: gardenia 4500g, turmeric 4500g, artificial musk 1125g, borneol 150g
[0068] 1. Take gardenia and turmeric decoction pieces, grind them into coarse powder respectively, mix them and put them into a multi-energy extraction tank, add 8 times the amount of water, and extract the volatile oil. After 6 hours, 14.31 g of volatile oil was collected.
[0069] 2. After the extraction of volatile oil, the medicinal liquid is first filtered and sucked into the storage tank. Add 9 times the amount of water (5 times, 4 times) to the medicinal residue, and decoct and extract twice, each time for 1.5 hours. The extract is first filtered and sucked into the above-mentioned In the storage tank, the medicinal liquid is centrifuged by a GQ-105 tubular separator, and after the supernatant is removed from the centrifuged liquid, it is adsorbed on a D4006 macroporous resin (20 mesh) column, and the flow rate is adjusted to 75ml / min (taking a 145*16cm column as an example ), wh...
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