Ultrahigh-glowing filament temperature and flame-retardant reinforced PBT (polybutylece terephthalate) composite material and preparation method thereof
A glow wire temperature, composite material technology, applied in the field of PBT composite material and its preparation, can solve the problems of high price, no value for widespread use, no product, etc., and achieves low cost, good application value and market prospect, easy-to-control effects
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Embodiment 1
[0023] Raw materials and ratio:
[0024] PBT: intrinsic viscosity 0.8Dl / g, 41%;
[0025] Brominated flame retardant: Decabromodiphenylethane, trade name: Yabao 8010, 13%;
[0026] Phosphorus nitrogen flame retardant: melamine and triphenyl phosphate are mixed at 1:1, 7%;
[0027] Inorganic flame retardant: aluminum hydroxide and magnesium hydroxide mixed in 1:1, 5%;
[0028] Toughening agent: ethylene-methyl acrylate copolymer, 2.5%;
[0029] Antioxidant: Ciba 1076, 0.4%;
[0030] Lubricant: OP wax, 1.1%;
[0031] Glass fiber: 990 glass fiber produced by Jushi Group Co., Ltd., 30%; the commercially available glass fiber product itself has been surface-treated, but this invention is treated with a coupling agent, coupling agent: γ-aminopropyltriethoxy Silane, domestic model: KH550, dosage: 1% of glass fiber weight. This surfactant is used in a small amount and is not included in the total amount of the formula.
[0032] Production method: Put the weighed plastics and add...
Embodiment 2
[0034] PBT: intrinsic viscosity is 0.95Dl / g, 47%;
[0035] Brominated flame retardant: brominated styrene, trade name: Yabao 7010, 15%;
[0036] Phosphorus nitrogen flame retardant: melamine, 8%;
[0037] Inorganic flame retardant: antimony trioxide, 6%;
[0038] Toughener: EPDM grafted maleic anhydride, 2.5%,
[0039] Antioxidant: a mixture of Ciba 1076 and Ciba 168 at a ratio of 1:1, 0.3%;
[0040] Lubricant: OP wax, 1.2%;
[0041] Glass fiber: 988A glass fiber produced by Jushi Group Co., Ltd., 20%; the surface of commercially available glass fiber is treated with a coupling agent, coupling agent: γ-aminopropyltriethoxysilane, domestic model: KH550, dosage: glass 1% of fiber weight.
[0042] Production method: Put the weighed plastics and additives into the high mixer and mix for 3 minutes to obtain a uniform mixture, then control the processing temperature of the twin-screw extruder at 230-245°C, the screw speed at 300 rpm, and place the mixture in A twin-screw extru...
Embodiment 3
[0044] PBT: Intrinsic viscosity is 1.0Dl / g, 28%;
[0045] Brominated flame retardant: bromotriazine, trade name: Dead Sea bromine FR245, 17%;
[0046] Phosphorus nitrogen flame retardant: melamine derivative MCA, 9%;
[0047] Inorganic flame retardant: magnesium hydroxide, 6%;
[0048] Toughening agent: ethylene-methyl acrylate copolymer, 3.5%;
[0049] Antioxidant: a mixture of Ciba 1076 and Ciba 168 at a ratio of 1:1, 0.3%;
[0050] Lubricant: EBS, 1.2%;
[0051] Glass fiber: 990 glass fiber produced by Jushi Group Co., Ltd., 35%; commercially available glass fiber without additional surface treatment.
[0052] Production method: Put the weighed plastics and additives into a high mixer and mix for 4 minutes to obtain a uniform mixture, then control the processing temperature of the twin-screw extruder at 230-245°C, the screw speed at 320 rpm, and place the mixture in A twin-screw extruder is used for granulation, and the product is obtained by adding 35% by weight of gl...
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