Single-component extrusion molding conductive rubber for electromagnetic shielding and preparation method of single-component extrusion molding conductive rubber
An extrusion molding and electromagnetic shielding technology is applied in the field of single-component conductive rubber materials for electromagnetic shielding and its preparation, which can solve the problems of increasing filling amount, single conductive powder form, and declining comprehensive performance.
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Embodiment 1
[0019]The dendritic silver-coated copper powder and silver-plated glass fiber with a silver content of 18wt% were stirred in alcohol for 2 hours to clean the powder impurities according to a certain ratio (1200g dendritic silver-coated copper powder and 200g silver-plated glass fiber), It was then dried in vacuo at 60°C for two hours. On this basis, the amine-based coupling agent methyldisilazineamine was used to stir for 2 hours, and after mixing evenly, put it in a vacuum drying oven and heat it to 120°C to remove the excess coupling agent on the surface. Add 500g of 10000mPa.s vinyl-containing polydimethylsiloxane to the vacuum meshing machine, add 175g of fumed white carbon black under vacuum at 65°C and stir for 2 hours, after mixing evenly, pass through the double planetary stirring equipment in turn Add 0.375g of acetylenic alcohol inhibitor ethynylcyclohexylalkynol, 3g of platinum catalyst and part of the treated conductive powder and mix evenly to make component 1. At...
Embodiment 2
[0023] The dendritic silver-coated copper powder and silver-plated glass fiber with a silver content of 18wt% were stirred in alcohol for 4 hours to clean the powder impurities according to a certain ratio (1531g dendritic silver-coated copper powder and 69g silver-plated glass fiber), It was then dried in vacuo at 80°C for two hours. On this basis, the amine-based coupling agent methyldisilazineamine was used to stir for 3 hours, after mixing evenly, it was placed in a vacuum drying oven and heated to 150°C to remove excess coupling agent on the surface. Add 500g of vinyl-containing polydimethylsiloxane of 20000mPa.s into the vacuum meshing machine, add 114g of fumed white carbon black under vacuum at 65°C and stir for 2 hours, after mixing evenly, pass through the double planetary stirring equipment in turn Add 0.45 g of acetylenic alcohol inhibitor ethynyl cyclohexanol acetylenic alcohol, 3.40 g of platinum catalyst and the treated conductive powder and mix evenly to make c...
Embodiment 3
[0025] The dendritic silver-coated copper powder and silver-plated glass fiber with a silver content of 20wt% were stirred in alcohol for 2 hours to clean the powder impurities according to a certain ratio (1526g dendritic silver-coated copper powder and 508g silver-plated glass fiber), It was then dried in vacuo at 60°C for two hours. On this basis, the amine-based coupling agent methyldisilazineamine was used to stir for 3 hours, and after mixing evenly, it was placed in a vacuum drying oven and heated to 120°C to remove excess coupling agent on the surface. Add 500g of vinyl-containing polydimethylsiloxane of 5000mPa.s into the vacuum meshing machine, add 210g of fumed silica under vacuum at 65°C and stir for 2 hours. Add 0.52g of acetylenic alcohol inhibitor ethynylcyclohexylalkynol, 3.15g of platinum catalyst and the treated conductive powder and mix evenly to make component 1. At the same time, add the treated Mix the conductive powder evenly to make component 2. Then ...
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