Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same
A technology of Ganoderma lucidum polysaccharide and extract, which is applied to cosmetic preparations, skin care preparations, pharmaceutical formulations, etc., can solve the problems of long decolorization time, large loss rate of polysaccharides, rough texture, etc., and achieves obvious moisturizing effect and pure color. White, fine-textured effect
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Embodiment 1
[0018] After taking 10g of Ganoderma lucidum fruiting body slices, add 100mL of distilled water, reflux the hot water at 75°C to extract once, add ethanol to the extract to make the final concentration of ethanol 60%, let it settle at 4°C for 10h, filter it with suction, and dry the precipitate at 40°C dry and pulverize to obtain Ganoderma lucidum polysaccharide powder.
[0019] Weigh 1g of Ganoderma lucidum polysaccharide powder, dissolve it in 500mL of water and mix to make a solution, add 5.01g of activated carbon, adjust the pH to 2.5, ultrasonically mix for 20s, let stand at 20°C for 20min, 4000r·min -1 Centrifuge for 10 min, and take the supernatant to obtain a colorless and transparent Ganoderma lucidum polysaccharide extract. The content of Ganoderma lucidum polysaccharide was determined by phenol sulfuric acid method, and the decolorization rate of Ganoderma lucidum polysaccharide was determined by measuring the OD of the sample before and after decolorization. 490nm...
Embodiment 2
[0021] After taking 10g of Ganoderma lucidum fruiting body slices, add 500mL of distilled water, reflux the hot water at 99°C to extract three times, add ethanol to the extract to make the final concentration of ethanol 90%, let stand at 25°C for 24h, filter with suction, and dry the precipitate at 60°C dry and pulverize to obtain Ganoderma lucidum polysaccharide powder.
[0022] Weigh 2.5g Ganoderma lucidum polysaccharide powder, dissolve it in 500mL water and mix to make a solution, add 15.075g activated carbon, adjust the pH to 4.5, ultrasonically mix for 60s, let stand at 40°C for 100min, 10000r·min -1 After centrifuging for 30 min, the supernatant was taken to obtain a colorless and transparent Ganoderma lucidum polysaccharide extract, with a decolorization rate of 99.5% and a polysaccharide retention rate of 66.6%.
Embodiment 3
[0024] 100 g of the decolorized ganoderma polysaccharide extract of Example 1, 25 g of propylene glycol, 0.1 g of triethanolamine and 0.05 g of propylparaben are made into the water phase, and then 4 g of mineral oil, 1 g of lanolin and 2 g of cetyl alcohol are made into the oil phase . Heat the oil phase and water phase respectively until dissolved, keep the temperature at 50°C, and keep the rotation speed at 320r·min -1 , slowly add the oil phase into the water phase, emulsify for 5 minutes, let stand and cool to room temperature to obtain hand cream.
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