Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same
The technology of Ganoderma lucidum polysaccharide and extract is applied in cosmetic preparations, skin care preparations, pharmaceutical formulations and other directions, can solve the problems of rough texture, large loss rate of polysaccharides, long decolorization time, etc., and achieves fine texture and pure white color. , Moisturizing effect is obvious
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Embodiment 1
[0018] After taking 10g Ganoderma lucidum fruit body slices, add 100mL distilled water, 75℃ hot water reflux extraction once, add ethanol to the extract to make the final concentration of ethanol 60%, 4℃ stand for precipitation for 10h, suction filtration, precipitation at 40℃ drying Dried and crushed to obtain Ganoderma lucidum polysaccharide powder.
[0019] Weigh 1g of Ganoderma lucidum polysaccharide powder and dissolve it in 500mL water and mix to make a solution, add 5.01g activated carbon, adjust the pH to 2.5, ultrasonically mix for 20s, and let stand at 20℃ for 20min, 4000r·min -1 Centrifuge for 10 min and take the supernatant to obtain a colorless and transparent Ganoderma lucidum polysaccharide extract. The content of Ganoderma lucidum polysaccharide is determined by phenol sulfuric acid method, and the decolorization rate of Ganoderma lucidum polysaccharide is determined by measuring the OD of the sample before and after decolorization. 490nm Finally, the decolorizati...
Embodiment 2
[0021] After taking 10g of Ganoderma lucidum fruit body slices, add 500mL distilled water and reflux with hot water at 99°C for 3 times. Add ethanol to the extract to make the final concentration of ethanol 90%. Leave it to settle at 25°C for 24h, filter with suction, and dry the precipitate at 60°C. Dried and crushed to obtain Ganoderma lucidum polysaccharide powder.
[0022] Weigh 2.5g of Ganoderma lucidum polysaccharide powder and dissolve it in 500mL water and mix to make a solution. Add 15.075g of activated carbon, adjust the pH to 4.5, ultrasonically mix for 60s, and let stand at 40℃ for 100min, 10000r·min -1 Centrifuge for 30 minutes, and take the supernatant to obtain a colorless and transparent Ganoderma lucidum polysaccharide extract with a decolorization rate of 99.5% and a polysaccharide retention rate of 66.6%.
Embodiment 3
[0024] The decolorized Ganoderma lucidum polysaccharide extract 100g, propylene glycol 25g, triethanolamine 0.1g and propylparaben 0.05g were prepared into the water phase, and then 4g mineral oil, 1g lanolin and 2g cetyl alcohol were prepared into the oil phase. . Heat the oil phase and water phase to dissolve separately, keep the temperature at 50℃ and keep the speed at 320r·min -1 , Slowly add the oil phase to the water phase, emulsify for 5 minutes, let stand and cool to room temperature to obtain a hand cream.
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