Preparation method of semiconductor wafer cutting blade material
A wafer and cutting edge technology, which is applied in the field of semiconductor wafer cutting edge material preparation, can solve the problems of long pickling time, high water consumption, low jet mill output, etc., and achieve good wafer cutting effect, Uniform particle size distribution and good high temperature resistance
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Embodiment 1
[0032] Embodiment 1 A kind of preparation method of semiconductor wafer cutting edge material, comprises the following steps:
[0033] (1) For raw material crushing, select green silicon carbide block materials with a purity of ≥99% and black silicon carbide block materials to mix according to a mass ratio of 18:1, carry out jaw crushing and sieve, and collect silicon carbide particle size sand with a particle size of ≤3mm;
[0034] (2) Wet ball milling and overflow classification are performed in the wet method frequency conversion ball mill classification device (see figure 1 ) for grinding and grading, add medium balls and silicon carbide particle size sand according to the weight ratio of medium ball: silicon carbide particle size sand of 4:1, the speed of the frequency conversion wet ball mill is 80rpm in the early stage of 0.5h, and the speed of 2h in the middle period is 100rpm. In the later stage 1.5h, the rotation speed is 120rpm, and the water intake is 600L / h; the ...
Embodiment 2
[0043] Embodiment 2 A kind of preparation method of semiconductor wafer cutting edge material, comprises the following steps:
[0044] (1) For raw material crushing, select green silicon carbide block material with a purity of ≥99% and black silicon carbide block material to mix according to a mass ratio of 19:1, carry out jaw crushing and sieve, and collect silicon carbide particle size sand with a particle size of ≤3mm;
[0045] (2) Wet ball milling and overflow classification adopt the same wet method frequency conversion ball mill classification device as in Example 1 for wet milling and classification. When grinding and classifying, the ratio of medium ball: silicon carbide grain size sand is 5:1 The weight ratio of medium balls and silicon carbide particle size sand is added. The speed of the variable frequency wet ball mill is 90rpm in the first 0.6h, 100rpm in the middle 1.9h, 150rpm in the later 1.6h, and the water intake is 500L / h;
[0046] (3) Pickling and vacuum de...
Embodiment 3
[0054] Embodiment 3 A method for preparing a cutting edge of a semiconductor wafer is basically the same as in Embodiment 1, except that in the step (2), the wet grinding is carried out by ordinary wet frequency conversion ball milling, and then the Commonly used hydraulic classifiers are used for classification to obtain silicon carbide powder slurry in the required particle size range.
[0055] The performance indexes of the obtained semiconductor wafer cutting edge material are shown in Table 4.
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